Current through Register Vol. 48, No. 51, June 17, 2024
Part 7037.3100 - ANALYSIS OF PETROLEUM CONTAMINATED SOIL SAMPLESSubpart 1.General requirements.All petroleum contaminated soil samples must be analyzed using a United States Environmental Protection Agency approved laboratory method or equivalent, unless an alternative method is specified in subpart 2.
Subp. 2.Specific analysis requirements.Specific laboratory analysis requirements are given in items A to E for selected parameters.
A. Analysis for the parameters of parameter code A in part 7037.0500, subpart 2, must be done using purge-and-trap laboratory methodology in conjunction with EPA method 8010, Minnesota Department of Health method 466A, or an equivalent gas chromatography method.B. Analysis for the parameters of parameter code B in part 7037.0500, subpart 2, must be done using purge-and-trap laboratory methodology in conjunction with EPA method 8020 or an equivalent gas chromatography method.C. Total petroleum hydrocarbons as gasoline, code D in part 7037.0500, subpart 2, must be done using the Wisconsin Department of Natural Resources Modified Gasoline Range Organics (GRO) method.D. Total petroleum hydrocarbons as fuel oil, code E in part 7037.0500, subpart 2, must be done using the Wisconsin Department of Natural Resources Modified Diesel Range Organics (DRO) method.E. PCBs, code H in part 7037.0500, subpart 2, must be done using EPA method 8080 or an equivalent gas chromatography method.Statutory Authority: MS s 116.07