Ariz. Admin. Code § tit. 9, ch. 14, art. 6, tbl. 6.2.C

Current through Register Vol. 30, No. 45, November 8, 2024
Table 6.2.C - Approved Methods and Method Fees for Waste Parameters

1. Microbiology of Waste

Description

Reference

Method/s

Fee Per Method

Coliforms, Total, by Membrane Filter

F

9132

$228

Coliforms, Total, by Multiple Tube Fermentation

F

9131

$228

2. Sample Preparation for Waste

Acid Digestion of Water

F

3005A

$7

Alkaline Digestion for Hex Chome

F

3060A

$7

Bomb Preparation Method for Solid Waste

F

5050

$7

EP for Oily Wastes

F

1330A

$76

EP Toxicity

F

1310B

$76

Microwave Assisted Digestions Multiple EP

F

F

3015A

$7

3051A

$7

3052

$7

3546

$7

1320

$152

Oils, Greases, and Waxes

F

3040A

$7

Oils

F

3031

$7

Sediments, Sludges, and Soils

F

3050B

$7

SPLP

F

1312

$303

TCLP

F

1311

$303

Total Metals

F

3010A

$7

3020A

$7

Total Recoverable in Water

F

3005A

$7

3. Inorganic Chemistry and Metals of Solid Waste

Aluminum

Ammonia

F

F and F13

A

6010C

$10

6020A

$26

7000B

$26

6010D

$10

6020B

$26

350.3

$39

Antimony

Arsenic

F

F and F13

F

6010C

$10

6020A

$26

7062

$76

7000B

$26

7010

$26

6010D

$10

6020B

$26

6010C

$10

6020A

$26

7010

$26

7061A

$76

7062

$76

7063

$76

F and F13

6010D

$10

6020B

$26

Barium

Beryllium

Boron

Bromide

F

F and F13

F

F and F13

F

6010C

$10

6020A

$26

7000B

$26

7010

$26

6010D

$10

6020B

$26

6010C

$10

6020A

$26

7000B

$26

7010

$26

6010D

$10

6020B

$26

6010C

$10

F and F13

6010D

$10

F

9056A

$26

9211

$39

Cadmium

Calcium

Cation-Exchange Capacity of Soils

F

F and F13

F

F and F13

F

6010C

$10

6020A

$26

7000B

$26

7010

$26

6010D

$10

6020B

$26

6010C

$10

6020A

$26

7000B

$26

6010D

$10

6020B

$26

9080

$34

9081

$34

Chloride

F

9056A

$26

9057

$76

9212

$39

9250

$76

9251

$76

9253

$39

Chlorine, Total, in New and Used Petroleum Products

F

9075

$76

9076

$39

9077

$39

Chromium, Hexavalent

F

7195

$26

7196A

$76

7197

$26

7198

$40

7199

$76

Chromium, Total

F

F and F13

6010C

$10

6020A

$26

7000B

$26

7010

$26

6010D

$10

6020B

$26

Cobalt

Compatibility Test for Wastes and Membrane Liners

F

F and F13

F

6010C

$10

6020A

$26

7000B

$26

7010

$26

6010D

$10

6020B

$26

9090A

$152

Copper

Corrosive to Steel

F

F and F13

F

6010C

$10

6020A

$26

7000B

$26

7010

$26

6010D

$10

6020B

$26

1110A

$63

Corrosivity pH Determination

F

9040C

$63

Cyanide

F

9010C

$13

9012B

$76

9213

$76

9014

$76

F9

9015

$76

Cyanide Extraction for Solids and Oils

F10

9013A

$39

Dermal Corrosion

F

1120

$63

Ignitability of Solids

F

1030

$32

Flash Point by Pensky Martems Cup

F

1010A

$32

Flash Point by Set-a Flash

F

1020B

$32

Fluoride

F

9056A

$26

9214

$39

Iron

Kjeldahl Total, Nitrogen

F

F and F13

A

6010C

$10

6020A

$26

7000B

$26

7010

$26

6010D

$10

6020B

$26

351.4

$76

Lead

Liquid Release Test Procedure

F

F and F13

F

6010C

$10

6020A

$26

7000B

$26

7010

$26

6010D

$10

6020B

$26

9096

$39

Lithium

Magnesium

F

F and F13

6010C

$10

7000B

$26

6010D

$10

F

F and F13

6010C

$10

6020A

$26

7000B

$26

6010D

$10

6020B

$26

Manganese

Mercury

Molybdenum

Nickel

Nitrate

F

F and F13

F

F and F13

F

F and F13

6010C

$10

6020A

$26

7000B

$26

7010

$26

6010D

$10

6020B

$26

6010C

$10

6020A

$26

7470A

$52

7471B

$52

7472

$152

7473

$152

7474

$152

6010D

$10

6020B

$26

6010C

$10

7000B

$26

7010

$26

6010D

$10

F

F and F13

F

6010C

$10

6020A

$26

7000B

$26

7010

$26

6010D

$10

6020B

$26

9210A

$39

9056A

$26

Nitrite

Oil and Grease and Petroleum Hydrocarbons

F

A4.24

9056A

$26

9216

$39

1664B

$76

O-Phosphate-P

F

9056A

$26

Osmium

F

7000B

$26

Paint Filter Liquids Test

F

9095B

$19

Perchlorate

pH (Hydrogen Ion)

A5

314.0

$76

F

6850

$152

F

9041A

$39

9045D

$39

Phosphorus

Phosphorus, Total

F

6010C

$10

F and F13

6010D

$10

A

365.3

$76

Potassium

Saturated Hydraulic and Leachate Conductivity and Intrinsic Permeability

F

F and F13

F

6010C

$10

6020A

$26

7000B

$26

6010D

$10

6020B

$26

9100

$152

Selenium

Silica Silver

Sodium

Sodium Azide

F

6010C

$10

6020A

$26

7010

$26

7741A

$26

7742

$76

F and F13

F

6010D

$10

6020B

$26

6010C

$10

F and F13

6010D

$10

F

F and F13

F

F and F13

C

6010C

$10

6020A

$26

7000B

$26

7010

$26

6010D

$10

6020B

$26

6010C

$10

6020A

$26

7000B

$26

6010D

$10

6020B

$26

4110C (2011)

$76

Specific Conductance

F

9050A

$39

Strontium

Sulfate

F

F and F13

6010C

$10

7000B

$26

6010D

$10

F

9035

$76

9036

$76

9038

$76

9056A

$26

Sulfides

F

9030B

$76

9031

$76

9034

$76

9215

$76

Thallium

Tin

Titanium

F

F and F13

F

F and F13

6010C

$10

6020A

$26

7000B

$26

7010

$26

6010D

$10

6020B

$26

6010C

$10

7000B

$26

6010D

$10

F

6010C

$10

Vanadium

Water

F

F and F13

F

6010C

$10

6020A

$26

7000B

$26

7010

$26

6010D

$10

6020B

$26

9000

$32

9001

$32

White Phosphorus by GC

F

7580

$116

Zinc

F

F and F13

6010C

$10

6020A

$26

7000B

$26

7010

$26

6010D

$10

6020B

$26

4. Organics Procedures in Waste

Separatory Funnel Liquid-Liquid Extraction

F

3510C

$13

Organic Compounds in Water by Microextraction

F5

3511

$13

Continuous Liquid-Liquid Extraction

F

3520C

$13

SPE

F

3535A

$13

Soxhlet Extraction

F

3540C

$13

Automated Soxhlet Extraction

F

3541

$13

Pressurized Fluid Extraction

F

3545A

$13

Ultrasonic Extraction

F

3550C

$13

Supercritical Fluid Extraction of Total Recoverable Petroleum Hydrocarbons

F

3560

$13

Supercritical Fluid Extraction of PAHs

F

3561

$13

SFE of PCBs and Organochlorine Pesticides

F

3562

$13

MSE

F4

3570

$13

Waste Dilution

F

3580A

$13

Waste Dilution for Volatile Organics

F

3585

$13

Alumina Cleanup

F

3610B

$13

Alumina Column Cleanup and Separation of Petroleum Wastes

F

3611B

$13

Florisil Cleanup

F

3620C

$13

Silica Gel Cleanup

F

3630C

$13

Gel-Permeation Cleanup

F

3640A

$13

Acid-Base Partition Cleanup

F

3650B

$13

Sulfur Cleanup

F

3660B

$13

Sulfuric Acid/Permanganate Cleanup

F

3665A

$13

Screening Solids for VOCs

F

3815

$76

Hexadecane Extraction and Screening for Purgeable Organics

F

3820

$76

Screening for Pentachlorophenol by Immunoassay

F

4010A

$76

Screening for 2,4-Dichlorophenoxyacetic Acid by Immunoas-say

F

4015

$76

Screening for PCBs by Immunoassay

F

4020

$76

Screening for PCDDs and PCDFs by Immunoassay

F3

4025

$76

Soil Screening for Petroleum Hydrocarbons by Immunoassay

F

4030

$76

Soil Screening for PAHs by Immunoassay

F

4035

$76

Soil Screening for Toxaphene by Immunoassay

F

4040

$76

Soil Screening for Chlordane by Immunoassay

F

4041

$76

Soil Screening for DDT by Immunoassay

F

4042

$76

TNT Explosives in Soil by Immunoassay

F

4050

$76

RDX in Soil by Immunoassay

F

4051

$76

Screening Environmental Samples for Planar Organic Compounds

F

4425

$76

Triazine Herbicides by Quantitative Immunoassay

F

4670

$76

VOCs in Various Sample Matrices Using Equilibrium Head-space Analysis

F8

5021A

$13

Purge-and-Trap for Aqueous Samples

F6

5030C

$13

Volatile, Nonpurgeable, Water-Soluble Compounds by Azeo-tropic Distillation

F

5031

$13

VOCs by Vacuum Distillation

F

5032

$13

Closed-System Purge-and-Trap and Extraction for Volatile Organics in Soil and Waste Samples

F2

5035A

$13

Analysis for Desorption of Sorbent Cartridges from VOST

F

5041A

$13

EDB and DBCP by Microextraction and GC

F

8011

$116

C10 - C32 Hydrocarbons

K

8015AZ 1

$116

Nonhalogenated Organics Using GC/FID

F7

8015D

$116

Aromatic and Halogenated Volatiles by GC Using Photoionization and/or Electrolytic Conductivity Detectors

F

8021B

$152

Acrylonitrile by GC

F

8031

$76

Acrylamide by GC

F

8032A

$76

Acetonitrile by GC with Nitrogen-Phosphorus Detection

F

8033

$76

Phenols by GC

F

8041A

$116

Phthalate Esters by GC/ECD

F

8061A

$116

Nitrosamines by GC

F

8070A

$116

Organochlorine Pesticides by GC

F

8081B

$152

Elemental Quantitation by GC/AED

F

8085

$116

PCBs by GC

F

8082A

$152

Nitroaromatics and Cyclic Ketones by GC

F

8091

$116

Explosives by GC

F

8095

$116

PAHs

F

8100

$116

Haloethers by GC

F

8111

$116

Chlorinated Hydrocarbons by GC: Capillary Column Technique

F

8121

$116

Aniline and Selected Derivatives by GC

F

8131

$116

Organophosphorus Compounds by GC

F

8141B

$152

Chlorinated Herbicides by GC Using Methylation or Pentafluo-robenzylation Derivatization

F

8151A

$152

VOCs by GC/MS, including n-Hexane VOCs by VD/GC/MS

F

8260B

$152

F12 and F13

8260C/8000D

$152

F

8261

$152

Semivolatile Organic Compounds by GC/MS

Semivolatile Organic Compounds (PAHs and PCBs) in Soils/ Sludges and Solid Wastes Using TE/GC/MS

F

8270C

$152

F and F13

8270D/8000D

$152

F

8275A

$152

8280A: Polychlorinated Dibenzo-p-Dioxins and PCDFs by HRGC/LRMS

F

8280B

$258

PCDDs and PCDFs by HRGC/HRMS

F

8290A

$258

PAHs

F

8310

$116

Determination of Carbonyl Compounds by HPLC

F

8315A

$116

Acrylamide, Acrylonitrile, and Acrolein by HPLC

F

8316

$116

N-Methylcarbamates by HPLC

F

8318A

$116

Solvent-Extractable Nonvolatile Compounds by HPLC/TS/MS or UV Detection

F

8321B

$152

Solvent Extractable Nonvolatile Compounds by HPLC/PB/MS

F

8325

$152

Nitroaromatics and Nitramines by HPLC

F

8330A

$116

Nitroaromatics, Nitramines, and Nitrate Esters

F11

8330B

$116

Tetrazene by Reverse Phase HPLC

F

8331

$116

Nitroglycerin by HPLC

F

8332

$116

GC/FT-IR Spectrometry for Semivolatile Organics: Capillary Column

F

8410

$116

Analysis of Bis (2-chloroethyl) Ether and Hydrolysis Products by Direct Aqueous Injection GC/FT-IR

F

8430

$116

Total Recoverable Petroleum Hydrocarbons by Infrared Spec-trophotometry

F

8440

$116

Screening for RDX/MDX in Soil

F

8510

$76

Colorimetric Screening Method for TNT in Soil

F

8515

$76

Screening for Total VOH in Water

F

8535

$76

PCP by UV Colorimetry

F

8540

$108

TOX

F

9020B

$76

POX

F

9021

$76

TOX by Neutron Activation Analysis

F

9022

$114

EOX in Solids

F

9023

$114

TOCs

F

9060A

$76

Phenolics

F

9065

$152

9066

$152

9067

$152

HEM for Aqueous Samples

F

9070A

$76

HEM for Sludge, Sediment, and Solid Samples

F

9071B

$76

Screening for TRPH in Soil

F

9074

$76

Screening for PCBs in Soil

F

9078

$76

Screening for PCBs in Oil

F

9079

$76

PCBs in Waste Oil

A4.28

600/4-81-045

$152

5. Bulk Asbestos Analysis of Waste

Bulk Asbestos Analysis Fiber Counting

A4.29

Bulk Asbestos

$228

G

9002

$228

G1 and A4.29

Bulk Asbestos

$228

G

7400

$228

7402

$228

6. Radiochemistry of Waste

Alpha-Emitting Radium Isotopes

F

9315

$206

Gross Alpha and Beta

F

9310

$206

Radium-228

F

9320

$206

Ariz. Admin. Code tit. 9, ch. 14, art. 6, tbl. 6.2.C

Adopted by final rulemaking at 22 A.A.R. 2683, effective 10/1/2016.