GIVAUDAN SADownload PDFPatent Trials and Appeals BoardSep 2, 20212020006064 (P.T.A.B. Sep. 2, 2021) Copy Citation UNITED STATES PATENT AND TRADEMARK OFFICE UNITED STATES DEPARTMENT OF COMMERCE United States Patent and Trademark Office Address: COMMISSIONER FOR PATENTS P.O. Box 1450 Alexandria, Virginia 22313-1450 www.uspto.gov APPLICATION NO. FILING DATE FIRST NAMED INVENTOR ATTORNEY DOCKET NO. CONFIRMATION NO. 15/515,857 03/30/2017 Emmanuel AUSSANT 102790-418 1024 27389 7590 09/02/2021 PARFOMAK, ANDREW N. NORRIS MCLAUGHLIN, PA 7 Times Square, 21st Floor NEW YORK, NY 10036-6524 EXAMINER PIPIC, ALMA ART UNIT PAPER NUMBER 1617 NOTIFICATION DATE DELIVERY MODE 09/02/2021 ELECTRONIC Please find below and/or attached an Office communication concerning this application or proceeding. The time period for reply, if any, is set in the attached communication. Notice of the Office communication was sent electronically on above-indicated "Notification Date" to the following e-mail address(es): anparfomak@norris-law.com jkelly@norris-law.com nmanfredi@norris-law.com PTOL-90A (Rev. 04/07) UNITED STATES PATENT AND TRADEMARK OFFICE BEFORE THE PATENT TRIAL AND APPEAL BOARD Ex parte EMMANUEL AUSSANT, ADDI FADEL, IAN MICHAEL HARRISON, CHRISTIAN QUELLET, EWELINA BURAKOWSKA-MEISE, WOLFGANG DENUELL, and THOMAS SOLTYS Appeal 2020-006064 Application 15/515,857 Technology Center 1600 Before TAWEN CHANG, TIMOTHY G. MAJORS, and JAMIE T. WISZ, Administrative Patent Judges. WISZ, Administrative Patent Judge. DECISION ON APPEAL Pursuant to 35 U.S.C. § 134(a), Appellant1 appeals from the Examiner’s decision to reject claims 1, 3, 5–8, 11–15, 17, and 18. We have jurisdiction under 35 U.S.C. § 6(b). We AFFIRM. 1 We use the word “Appellant” to refer to “applicant” as defined in 37 C.F.R. § 1.42. Appellant identifies Givaudan, SA as the real party in interest. Appeal Br. 1. Appeal 2020-006064 Application 15/515,857 2 CLAIMED SUBJECT MATTER The Specification describes “encapsulated perfume compositions, comprising one or more core-shell capsules, wherein the core contains a perfume and the shell contains a polyurea resin (‘polyurea capsules’).” Spec. 1. According to the Specification, “by employing hydroxyethylcellulose as a dispersing aid, it was possible to form, in a straightforward manner, an encapsulated perfume composition, in the form of a slurry in which polyurea capsules were stably dispersed, and which possessed an acceptable viscosity.” Id. at 2. Claim 1, the only independent claim, is illustrative of the claimed subject matter and is reproduced below: 1. An encapsulated perfume composition in the form of an aqueous slurry comprising one or more core-shell capsules, each having a core and a shell, dispersed in an aqueous dispersing medium, wherein the core contains a perfume and the shell contains a polyurea resin, and wherein the one or more core-shell capsules are in the form of a suspension, which upon visual inspection, shows no sign of phase separation such as creaming, settling, precipitation or coagulation when stored for a period of 2 weeks at a temperature of 50°C, the suspension having a viscosity of up to 3000 centipoise, when measured on a rheometer using rotating disks at a shear rate of 21 s-1 at a temperature of 25°C, and wherein the aqueous dispersing medium contains a hydroxyethyl cellulose dispersing aid which is present in an amount of 0.05%wt. to 1.0%wt. based on the total weight of the slurry. Appeal Br. 24 (Claims App.). Appeal 2020-006064 Application 15/515,857 3 REJECTIONS The Examiner rejected claim 18 under 35 U.S.C. § 112 as failing to comply with the written description requirement. The Examiner rejected claims 1, 3, 5–8, 11–15, 17, and 18 under 35 U.S.C. § 103 as being unpatentable over Lei2 and Dihora.3 ISSUES AND ANALYSIS Rejection of claim 18 under 35 U.S.C. § 112(a) The Examiner rejected claim 18 as failing to comply with the written description requirement. Final Act. 3. Claim 18 recites the composition of claim 1, wherein the composition excludes solvents in the aqueous dispersing medium. Appeal Br. 26. The Examiner finds that the Specification does not describe embodiments where solvent is present or absent from the aqueous dispersing phase. Final Act. 3. Appellant cites to page 4, lines 14–15 of the Specification which state that, “[t]he hydrophobic phase may also include suitable solvents, although, in a preferred aspect of the present invention, no solvents are employed,” for support. Id. However, the Examiner finds that this sentence does not provide sufficient support for a limitation that requires excluding solvents from the aqueous dispersing medium. Id. The Examiner also finds that the application supports excluding solvents from the hydrophobic phase and the core of the capsule but does not describe embodiments where solvent is present or absent from the aqueous dispersing phase. Id. 2 Lei et al., US 2011/0071064 A1, published Mar. 24, 2011 (“Lei”) 3 Dihora et al., US 2011/0268778 A1, published Nov. 3, 2011 (“Dihora”). Appeal 2020-006064 Application 15/515,857 4 Appellant does not respond to this rejection in the Appeal Brief. See Appeal Br. 1–23. Appellant has not provided any express argument responding to the Examiner’s rejection and, on this record, has not therefore demonstrated error in the Examiner’s finding that the Specification lacks an adequate written description for the subject matter of claim 18. Therefore, we affirm the Examiner’s rejection of claim 18 as lacking written description support. Rejection of claims 1, 3, 5–8, 11–15, 17, and 18 under 35 U.S.C. § 103 as being unpatentable over Lei and Dihora The Examiner finds that Lei teaches products for washing and cleaning surfaces that comprise micro-encapsulated benefit agents including polyurea microcapsules. Final Act. 4 (citing Lei, Abstract). The Examiner also finds that Lei teaches preparation of polyurea capsules of encapsulated fragrance in example 4 and the resulting composition is described as a slurry. Id. (citing Lei ¶¶ 128, 178). The Examiner further finds that example 17 describes methods of making slurry compositions comprising dispersants and capsule slurries of example 4 and that these compositions were measured to have viscosities of 986 cp and 17 cp. Id. (citing Lei ¶¶ 155– 157). The Examiner finds that Lei teaches incorporating carboxymethyl cellulose as a suspending agent in a slurry. Id. at 5 (citing Lei ¶¶ 31, 32). The Examiner acknowledges that Lei does not teach a hydroxyethyl cellulose dispersing aid but finds that this limitation is suggested by Dihora. Id. at 5. The Examiner finds that Dihora teaches compositions comprising encapsulated benefit agents such as perfumes, wherein the compositions comprise suspending agents at a concentration effective for suspending water-insoluble materials at concentration ranges from about 0.1 to 10%. Id. Appeal 2020-006064 Application 15/515,857 5 (citing Dihora, Abstract, ¶¶ 8, 56, 176). The Examiner also finds that Dihora discloses suspending agents including hydroxyethyl cellulose, carboxymethyl cellulose, and polyvinyl alcohol. Id. (citing Dihora ¶ 177). According to the Examiner, it would have been obvious to a person of ordinary skill in the art “to have formulated a stable slurry by combining Lei’s capsules from example 4 with the suspending agent carboxymethyl cellulose in a concentration of 0.1 to 5%, with a reasonable expectation of success because Lei teaches formulating a slurry with carboxymethyl cellulose as a suspending agent in a concentration of 0.1 to 5%.” Id. at 5 (citing Lei ¶¶ 31, 32). The Examiner further finds that a person of ordinary skill in the art “would have been motivated to use a suspending agent [in Lei’s compositions] because the purpose of Lei is to form a stable slurry composition[,] and [Lei] teaches that suspending agents are useful for forming a stable slurry composition.” Id. The Examiner concludes that “[i]t would have been further obvious to have modified Lei by replacing carboxymethyl cellulose with hydroxyethyl cellulose, with a reasonable expectation of success in obtaining a microcapsule suspension because it was known from Dihora that carboxymethyl cellulose and hydroxyethyl cellulose are equally suitable as suspending agents in aqueous suspensions of microcapsules.” Id. Regarding the viscosity limitations, the Examiner finds that the compositions of Example 17 are described as having viscosities of 17 cp and 986 cp. Id. at 6. According to the Examiner, it would have been obvious to an ordinarily skilled artisan “to have formulated [the] composition in example 4 as a flowable slurry of capsules, with a reasonable expectation of success because Lei teaches that a slurry of capsules has to be flowable in Appeal 2020-006064 Application 15/515,857 6 order to be usable and describes 17 cp and 986 cp as suitable viscosities.” Id. The Examiner also finds that, while Lei does not describe the effect of storage conditions of 2 weeks at a temperature of 50ºC on the capsule slurries, “since the prior art slurries are structurally identical to the claimed slurries, it would have been obvious to a person of ordinary skill in the art to conclude that the prior art slurries would have had the same properties as presently claimed slurries when placed under identical conditions.” Id. at 7. Appellant argues that example 4 of Lei does not disclose the claimed stability properties of the capsule slurry after 2 weeks at 50ºC. Appeal Br. 11. According to Appellant, Lei is “completely silent” on how to achieve these stability requirements and the Examiner is impermissibly picking and choosing amongst Lei’s teachings. Id. Appellant also argues that Lei does not disclose hydroxyethyl cellulose and does not include a reasonable suggestion to use carboxyethyl cellulose absent an impermissible hindsight reconstruction. Id. at 14. With regard to viscosity, Appellant argues that Lei requires “a ‘[synergistic]’ mixture of two dispersants, specifically a polyvinyl alcohol (PVA, Mowiol 3-83) with an anionic dispersant Morwet D-425 (a naphthalene sulfate)” and that both “were shown to be necessary to form a stable free-flowing slurry with very low viscosity.” Appeal Br. 15. Appellant contends that a “skilled artisan, seeking to provide stable, low viscosity slurries would not ‘break’ the synergistic [combination] of a polyvinyl alcohol (PVA, Mowiol 3-83) with an anionic dispersant Morwet D-425 (a naphthalene sulfate) as such would be expected to defeat the success of Lei's compositions.” Id. Appellant concludes that, “no Appeal 2020-006064 Application 15/515,857 7 consideration of Lei even with ancillary consideration of Dihora, motivate a skilled artisan to abandon Lei’s teaching of a necessary and synergistic composition of dispersants and to seek a different material, with any [reasonable] expectation of success.” Id. at 17. Appellant further contends that “nothing in Dihora suggests the selection of hydroxyethyl cellulose for the production of [a] stable suspension of microcapsules without leading to an undesired increase in viscosity” and that Dihora also does not discuss polyurea containing shells of microencapsulated materials. Id. at 17–18. According to Appellant, the skilled artisan would need to engage in undue experimentation to optimize any formulation that possessed the claimed properties. Id. at 18. Appellant also asserts that their Specification “demonstrate[s] the surprising nature of using hydroxyethyl cellulose in forming aqueous slurries containing encapsulated materials wherein the encapsulating shell includes a polyurea resin.” Id. at 19–20. According to Appellant, the properties of the claimed aqueous slurries were unexpected as shown in Table 8. Id. at 20–21. According to Appellant, “[s]urprisingly, only with hydroxyethyl cellulose (entry B) - but not with any of the modified starches or acrylate copolymers (entries A, C, G and G) - was phase separation avoided, to the degree recited in the claims.” Id. at 22. We find that the Examiner has the better position. Lei discloses compositions including micro-encapsulated benefit agents that may include perfumes. Lei, Abstract, ¶ 50. Lei also discloses that a dispersant can be used to make the formulation stable. Id. ¶ 27 (“The emulsifier or dispersant can be used alone and together in the invention as long as stable capsule formulation is obtained.”). Lei discloses the use of a “wide range of Appeal 2020-006064 Application 15/515,857 8 dispersant[s]” including carboxymethyl cellulose and also discloses that the dispersant concentration can range from 0.1% to 5%, preferably from 0.25% to 2%. Id. ¶¶ 31, 32. Example 4 of Lei discloses the preparation of a polyurea capsule with a full fragrance and describes the composition as a “capsule slurry.” Id. ¶¶ 127, 128. Lei also teaches that “[o]ne of the key physical characteristic[s] of a suspension such as a capsule slurry is its viscosity. For the capsule slurry to be usable, it has to be flowable.” Id. ¶ 155. Example 17 of Lei discloses the generation of capsule slurries with dispersants using the procedures of Example 4, wherein such slurries had viscosities of 986 cp and 17 cp. Id. ¶¶ 156–157. Dihora discloses compositions comprising encapsulated benefit agents for perfume delivery. Dihora, Abstract. Dihora also discloses that its compositions comprise suspending agents at a concentration effective for suspending water-insoluble materials, in a range from about 0.1 to 10%. Id. ¶ 176. Dihora discloses use of suspending agents such as carboxymethyl cellulose, hydroxyethyl cellulose, and polyvinyl alcohol. Id. ¶ 177. We agree with the Examiner that it would have been obvious to a person of ordinary skill at the time of the invention to have formulated a stable slurry using the methods described in Examples 4 and 17 of Lei along with a dispersant/suspending agent such as carboxymethyl cellulose in a concentration of 0.1–5%, preferably 0.25–2%. See Lei ¶¶ 31, 32, 127–128, 155–157. It also would have been obvious to substitute the carboxymethyl cellulose of Lei with the hydroxyethyl cellulose disclosed in Dihora with a reasonable expectation of success because carboxymethyl cellulose and hydroxyethyl cellulose were both described as suitable suspending agents in Dihora. Dihora ¶¶ 176–177. It is obvious to those skilled in the art to Appeal 2020-006064 Application 15/515,857 9 substitute one known equivalent for another. See In re Omeprazole Patent Litigation, 483 F.3d 1364, 1374 (Fed. Cir. 2007) (“[T]his court finds no . . . error in [the] conclusion that it would have been obvious to one skilled in the art to substitute one ARC [alkaline reactive compound] for another.”). Appellant argues that Lei does not disclose the use of hydroxyethyl cellulose; however, this disclosure is supplied by Dihora. Appellant also argues that Dihora does not discuss polyurea containing shells of microencapsulated materials; however, this disclosure is supplied by Lei. Appeal Br. 13, 18, 19. “Non-obviousness cannot be established by attacking references individually where the rejection is based upon the teachings of a combination of references. [The reference] must be read, not in isolation, but for what it fairly teaches in combination with the prior art as a whole.” In re Merck & Co., 800 F.2d 1091, 1097 (Fed. Cir. 1986). Based on the disclosures of Lei and Dihora discussed above, we are not persuaded that the Examiner used impermissible hindsight. “Any judgment on obviousness is in a sense necessarily a reconstruction based upon hindsight reasoning, but so long as it takes into account only knowledge which was within the level of ordinary skill at the time the claimed invention was made and does not include knowledge gleaned only from applicant’s disclosure, such a reconstruction is proper.” In re McLaughlin, 443 F.2d 1392, 1395, 170 USPQ 209, 212 (CCPA 1971). Lei discloses the formulation of stable polyurea capsule slurries and the use of dispersants such as carboxymethyl cellulose and polyvinyl alcohol to produce desired viscosities. Dihora also discloses encapsulated benefit agents and the use of dispersants/suspending agents including hyrdroxyethyl cellulose, carboxymethyl cellulose, and polyvinyl alcohol. Here, the use of Appeal 2020-006064 Application 15/515,857 10 hydroxyethyl cellulose as a dispersant in the compositions of Lei is no “more than the predictable use of prior art elements according to their established functions.” KSR Int’l Co. v. Teleflex Inc., 550 U.S. 398, 417 (2007). Appellant also argues that Lei does not disclose the claimed stability properties after 2 weeks at 50ºC. Appeal Br. 11. However, we agree with the Examiner that, because the properties of Lei’s composition, in combination with the use of hydroxyethyl cellulose disclosed in Dihora, includes all the structural claim limitations, it is presumed to have the same claimed stability properties. “From the standpoint of patent law, a compound and all of its properties are inseparable; they are one and the same thing.” In re Papesch, 315 F.2d 381, 391 (CCPA 1963). After a prima facie case is made out, the burden shifts to the applicant to show a difference between the prior art compositions and the claimed compositions. The Patent Office lacks the resources to do comparisons. In re Best, 562 F.2d 1252, 1255. Appellant has not provided any reasons why the compositions suggested by the prior art would not possess the claimed stability properties, but merely argues that such properties are not explicitly disclosed. Appellant also appears to argue that Lei teaches away from using anything other than the “synergistic” combination of polyvinyl alcohol (PVA, Mowiol 3–83) with an anionic dispersant Morwet D–425 (a naphthalene sulfate) because such combination is taught to be effective in Example 17 of Lei. See Appeal Br. 15. We disagree. While Example 17 of Lei demonstrates a synergistic effect when combining two different polymeric dispersants (Morwet D–425 and Mowiol 3–83), the disclosure of Lei is not limited to using just these two dispersants. In fact, Lei teaches that Appeal 2020-006064 Application 15/515,857 11 a “wide range” of dispersants can be used, including carboxymethyl cellulose (which, as discussed above, could be substituted with hydroxyethyl cellulose based on the teachings of Dihora). A teaching away requires a reference to actually criticize, discredit, or otherwise discourage the claimed solution. See In re Fulton, 391 F.3d 1195, 1201 (Fed. Cir. 2004) (“The prior art’s mere disclosure of more than one alternative does not constitute a teaching away from any of these alternatives because such disclosure does not criticize, discredit, or otherwise discourage the solution claimed.”). With respect to Appellant’s asserted evidence of unexpected results, we find that Appellant has not compared their results to the closest prior art. “To be particularly probative, evidence of unexpected results must establish that there is a difference between the results obtained and those of the closest prior art, and that the difference would not have been expected by one of ordinary skill in the art at the time of the invention.” Bristol-Myers Squibb Co. v. Teva Pharm. USA, Inc., 752 F.3d 967, 977 (Fed. Cir. 2014). In this case, Lei teaches polyurea capsules with fragrance including the dispersants 0.5% Morwet D–425 (a naphthalene sulfonate) and Mowiol 3–83 (a polyvinyl alcohol). Lei ¶¶ 127–128, 155–157. Appellant has not shown how their results compare to the compositions disclosed in Lei, which were shown to have viscosities falling within the claimed range of less than 3000 centipoise. We also agree with the Examiner that the data presented by Appellant is not commensurate in scope with the claims. “The evidence presented to rebut a prima facie case of obviousness must be commensurate in scope with the claims to which it pertains.” In re Dill, 604 F.2d 1356, 1361 (CCPA 1979). First, the slurries in Table 8 vary by type of dispersant used as well Appeal 2020-006064 Application 15/515,857 12 as by wt % of dispersant. Spec. 35. Thus, it is not clear whether the resulting viscosity is based on the type of dispersant or on the concentration of such dispersant. Further, claim 1 recites that the dispersant is present in an amount from 0.05 to 1.0% wt. Here, Appellant presents data to show unexpected results for only a single wt % (0.4 wt %). Id. This one data point is not enough to show that any alleged unexpected results would occur for other compositions falling within the scope of the claims. Therefore, for the reasons above, we affirm the Examiner’s rejection of claim 1 as being obvious over Lei and Dihora. Claims 3, 5–8, 11–15, 17, and 18 are not argued separately apart from the independent claim, and, therefore, fall with claim 1. See 37 C.F.R. § 41.37(c)(1)(iv). CONCLUSION For the reasons described herein and those already of record, we affirm the Examiner’s rejection of claims 1, 3, 5–8, 11–15, 17, and 18. DECISION SUMMARY In summary: Claim(s) Rejected 35 U.S.C. § Reference(s)/Basis Affirmed Reversed 18 112(a) Written Description 18 1, 3, 5–8, 11–15, 17, 18 103 Lei, Dihora 1, 3, 5–8, 11–15, 17, 18 Overall Outcome 1, 3, 5–8, 11–15, 17, 18 Appeal 2020-006064 Application 15/515,857 13 No time period for taking any subsequent action in connection with this appeal may be extended under 37 C.F.R. § 1.136(a). See 37 C.F.R. § 1.136(a)(1)(iv). AFFIRMED Copy with citationCopy as parenthetical citation