Ex Parte Trummer et alDownload PDFPatent Trial and Appeal BoardFeb 21, 201912515090 (P.T.A.B. Feb. 21, 2019) Copy Citation UNITED STA TES p A TENT AND TRADEMARK OFFICE APPLICATION NO. FILING DATE FIRST NAMED INVENTOR 12/515,090 05/15/2009 Stefan Trummer 2352 7590 02/25/2019 OSTROLENK FABER LLP 845 THIRD A VENUE NEW YORK, NY 10022 UNITED STATES DEPARTMENT OF COMMERCE United States Patent and Trademark Office Address: COMMISSIONER FOR PATENTS P.O. Box 1450 Alexandria, Virginia 22313-1450 www .uspto.gov ATTORNEY DOCKET NO. CONFIRMATION NO. P/746-41 (V 12096) 6283 EXAMINER GREENE, NAN A ART UNIT PAPER NUMBER 1619 NOTIFICATION DATE DELIVERY MODE 02/25/2019 ELECTRONIC Please find below and/or attached an Office communication concerning this application or proceeding. The time period for reply, if any, is set in the attached communication. Notice of the Office communication was sent electronically on above-indicated "Notification Date" to the following e-mail address(es): pat@ostrolenk.com PTOL-90A (Rev. 04/07) UNITED STATES PATENT AND TRADEMARK OFFICE BEFORE THE PATENT TRIAL AND APPEAL BOARD Ex parte STEP AN TRUMMER, MICHAEL BECKER, and THOMAS SCHLEGL Appeal2017-006755 Application 12/515,090 Technology Center 1600 Before FRANCISCO C. PRATS, DEBORAH KATZ, and TIMOTHY G. MAJORS, Administrative Patent Judges. MAJORS, Administrative Patent Judge. DECISION ON APPEAL Appellants 1 submit this appeal under 35 U.S.C. § 134(a) involving claims to platelet-like pigments having a narrow thickness distribution. The Examiner rejected the claims as obvious and for obviousness-type double patenting. We have jurisdiction under 35 U.S.C. § 6(b). We reverse the rejection for obviousness, but affirm the rejection for obviousness-type double patenting. 1 Appellants identify the Real Party in Interest as Eckart GmbH. App. Br. 2. Appeal2017-006755 Application 12/515,090 STATEMENT OF THE CASE Appellants' "invention relates to thin platelet-like aluminum pigments having a narrow thickness distribution." Spec. 1 :4--5. According to the Specification, "[p ]latelet-like aluminum pigments are effect pigments and are distinguished by their unique metallic appearance and their high covering power." Id. at 1 :7-8. The Specification explains that, to create favorable properties ( e.g., metallic effect and brightness) in pigments, many factors are important, including "orientation, their size and size distribution," among others. Id. at 1:8-15. The Specification further explains that "so- called 'PVD pigments"' provide favorable characteristics such as brilliance and high gloss, but that such pigments also have drawbacks, such as "extremely high production costs."2 Id. at 2:7-10, 3: 1-2. According to the Specification, "[i]t has been found, very surprisingly, that the aluminum pigments of the invention have a metallic gloss [in applications] which has hitherto not been achieved in conventional pigments prepared by wet grinding, but has only been possible with PVD pigments." Id. at 10: 9-12. The Specification further discloses that, where "an almost mirror-like effect is observed when PVD pigments are used ... [,] [ s ]urprisingly, a similar effect can be achieved with the aluminum effects of the invention," which effect the Specification states is likely due to "[t]he small overall thickness of the pigments and the small breadth of thickness distribution." Id. at 10:13-19. 2 The Specification contrasts PVD pigments with another class of aluminum pigments ("so-called 'silver dollar pigments"') that are prepared by wet grinding of aluminum shot. Spec. 2:7-10. 2 Appeal2017-006755 Application 12/515,090 Claims 1-3, 5-16, and 36-38 are on appeal. Claim 1, the only independent claim, is illustrative and is reproduced below: 1. Platelet-like aluminum pigments having a narrow thickness distribution and at least partially coated with lubricant, wherein the pigments have a) a mean thickness hso of from 15 nm to 75 nm as determined by scanning electron microscope thickness count, b) a relative breadth of thickness distribution L'ih of from 30 % to less than 70 %, as determined by a scanning electron microscope thickness count and as calculated on the basis of the corresponding cumulative breakthrough curve of the relative frequencies of occurrence, according to the formula L'ih = 1 OOx(h90-h10) / hso, and c) an X-ray diffractogram, measured on pigments in substantially plane parallel orientation, having one or two main peaks which do not correspond to the [ 111] reflexes, wherein the platelet-like aluminum pigments are produced by a method comprising (1) providing aluminum shot exhibiting a particle size distribution having a dshot, 10< 0.6 µm, a dshot, so< 2.0 µm and a dshot, 90 < 4.0 µm, wherein the aluminum shot is prepared in an atomizer by atomization of liquid aluminum, and (2) grinding the aluminum shot as defined in (1) above using a grinder in the presence of solvent and lubricants and grinding media having an individual weight of from 1.2 mg to 13 mg. App. Br. 12 (Claims App.). The claims stand rejected as follows: 3 Appeal2017-006755 Application 12/515,090 Claims 1-3, 5-16, and 36-38 under 35 U.S.C. § I03(a) as obvious over Minami, 3 Wheeler '0794 in view of Schlegl, 5 Wheeler, 6 and as optionally evidenced by Valimet. 7 See Ans. 2; Non-Final Rejection (dated Jan. 22, 2016) 3-11 (hereafter "Non-Final Act."). Claims 1-3, 5-16, and 36-38 for obviousness-type double patenting over the '832 patent8 in view of Minami, Wheeler '079, and Wheeler. An oral hearing before the Board took place on February 5, 2019. A transcript of that hearing will be entered in the prosecution record. DISCUSSION Obviousness-35 USC§ 103(a) Claim 1 The issue on appeal is whether a preponderance of the evidence cited by the Examiner establishes that claim 1 would have been obvious over the cited references. The Examiner finds that Minami "teaches aluminum flake pigments having excellent metallic luster and an average thickness (h50) in the range of 0.025 to 0.08 µm (i.e. 25-80 nm)," as well as a low-cost manufacturing process that includes grinding with steel balls in the presence of an organic 3 Minami, EP 1621586 Al, published Feb. 1, 2006. 4 Wheeler, US 2010/0167079 Al, published July 1, 2010. 5 Thomas Schlegl et al., US 2007/0199478 Al, published Aug. 30, 2007. 6 Ian Wheeler, Metallic Pigments in Polymers, Rapra Technology Limited 11-53 (1999). 7 Valimet Inc., Spherical Aluminum Powder, Rev. 1.1, published Mar. 20, 2006. The Examiner does not include, in the rejection on appeal or in the Answer, any findings specific to Valimet. So, that reference is not considered further in this Decision. 8 Maennig et al., US 8,333,832 B2, issued Dec. 18, 2012. 4 Appeal2017-006755 Application 12/515,090 solvent. Non-Final Act. 4; see, e.g., Minami ,r,r 17, 49--51 (Example 1). According to the Examiner, however, Minami "does not expressly disclose the instantly claimed span (i.e. relative breadth of thickness distribution L'ih), or the X-ray diffractogram for the resulting aluminum pigment." Non-Final Act. 4. With respect to the "wherein" clause of claim 1, which recites that the "pigments are produced by a method comprising," inter alia, providing aluminum shot having a particular particle size distribution, the Examiner turns to Wheeler '079. Non-Final Act. 7. More specifically, the Examiner cites a teaching in Wheeler that "[ t ]here is a need for a metal powder that has both low median particle diameter and a narrow particle size distribution," and that, by using such a metal powder in preparation of metal flake pigments "a substantially monodisperse metal flake pigment product may be obtained in virtually 100% yield." Id. (quoting Wheeler '079 ,r 15 (emphasis omitted)); see also Non-Final Act. 6 (citing the Wheeler publication regarding processes for manufacturing aluminum flake pigments from atomized aluminum powder). According to the Examiner, one "would clearly have been motivated to use a narrow size distribution of the aluminum shot starting material in order to obtain a more uniform platelet- like [appearance]," in view of Wheeler '079. Non-Final Act. 10. The Examiner also cites Schlegl as teaching aluminum pigments with a narrow distribution of thickness. Non-Final Act. 7-8. According to the Examiner, "[t]he only difference between the teachings of SCHLEGL and the instant application appears to be the relative breadth of thickness distribution L'ih (i.e. the span)." Id. at 8. Yet, the Examiner asserts, by adjusting speeds of rotation for milling the pigments, the ordinarily skilled 5 Appeal2017-006755 Application 12/515,090 person would have arrived at pigments with a L'ih of from 30-70% as claimed. Id. at 9. The Examiner then concludes it would have been obvious "to produce a platelet-like aluminum pigment starting with aluminum shot having a narrow size distribution, and using a ball mill and adjusting the parameters according to the knowledge in the art pertaining to ball mill pigment production." Non-Final Act. 10. According to the Examiner, a motivation to produce different grades of pigment, and using aluminum shot with a narrow size distribution, comes from "the economics and coloristic attractiveness of the product." Id. at 11. The Examiner asserts that "aluminum shot having a narrow size distribution ... was known at the time of the claimed invention and it would have been obvious to select as a suitable aluminum shot material such as suggested by WHEELER ['079]." Id. The Examiner further asserts that there would be a reasonable expectation of success in arriving at the claimed subject matter because adjusting parameters for pigment production is "considered within the ordinary skill in the art." Id. At the outset, Appellants contend that "[i]ndependent claim 1 ... is written in a product-by-process format." App. Br. 5; see also Non-Final Act. 13 (Examiner agreeing that "[t]he claim is constructed as a product-by- process claim"). According to Appellants, the claimed invention recognizes the importance of ( and obtains "unexpectedly improved results with") pigments that have a relatively narrow breadth of thickness distribution and that are produced from aluminum shot having a relatively narrow particle size distribution. App. Br. 5. Appellants argue that Minami, on the other hand, is concerned with average diameters and average thicknesses, which, Appellants note, are different particle parameters than thickness and particle 6 Appeal2017-006755 Application 12/515,090 size distributions. Id. Appellants contend that Minami "does not provide any motivation at all to either optimize the particle size distribution or the thickness distribution of the flakes." Id. at 6. Second, Appellants contend that Minami ( and the claims) require the use of atomized aluminum powder as the starting material. Id. at 7. According to Appellants, Wheeler '079 discloses that producing atomized aluminum powder in high yields is technically difficult and poses other limitations and challenges. Id. (citing Wheeler '079 ,r,r 6-9); see, e.g., Wheeler '079 ,r 6 ( describing "a possibility of explosion" when atomizing reactive metals, such as aluminum), ,r 8 ("The second characteristic exhibited by conventional atomisation processes is the generation of powder with a wide particle size distribution"); see also id. (Table 1 (illustrating a typical distribution)). So, Appellants argue, Wheeler '079 teaches preparing pigments using starting materials produced, not via atomization of aluminum as in claim 1, but with a "jetting process wherein molten metal is rejected [sic] from a jet head." App. Br. 7. According to Appellants, Wheeler '079 therefore teaches away from the present invention. 9 Appellants further contend that, even with the particle distributions described in Wheeler '079, those distributions are substantially different than what is claimed. Id. at 8. For example, Appellants highlight that only 0.22% of the particles in Wheeler have a size less than 4 µm, nowhere near 9 Appellants also argue, as allegedly evidenced by the June 12, 2015 Declaration of Dr. Stefan Engel ( along with the attachment to that declaration)), that Wheeler '079 is not enabled for the jetting of molten aluminum. App. Br. 7. As Appellants argue, and Dr. Engel opines, the high melting temperature of aluminum (roughly 660°C) would not work with, and indeed would melt, the piezoelectric jetting mechanisms described in Wheeler '079. Id.; see also Engel Deel. ,r,r 7-15. 7 Appeal2017-006755 Application 12/515,090 the requirement in claim 1 that 90% of the aluminum shot particles in the distribution have a size under 4 µm. Id. ( dshot, 90 < 4.0 µm in the claims). Id. Appellants also argue that the thickness distribution in Schlegl is not the thickness distribution as claimed - L'ih from 30 % to less than 70 %. To the contrary, Appellants contend, Schlegl discloses that the L'ih is between 70-140%, and "thus teaches away from the present invention." App. Br. 8. Moreover, Appellants contend, the other cited references do not provide an adequate disclosure of the pigments' thickness distribution that is claimed, or an adequate reason to modify that parameter. Id. at 9. In addition to the above, Appellants also argue that they have provided evidence of unexpected results in terms of the recited pigments' optical properties. Id. at 1 O; see Trummer Deel. ( dated Dec. 21, 2015), ,r 21; Spec. 33:20-24, 36:16-37:3. Upon considering the Examiner's findings and assertions related to the cited prior art, and Appellants' argument in response, we are not persuaded on this record that the Examiner met the burden to establish a prima facie case of obviousness. In re Oetiker, 977 F.2d 1443, 1445 (Fed. Cir. 1992) (The Examiner "bears the initial burden ... of presenting a prima facie case of unpatentability."). We explain further below. Appellants and the Examiner appear to agree that claim 1 is a product- by-process claim. With product-by-process claims, the manner in which the product is made is, as a legal matter, generally not limiting. In re Thorpe, 777 F .2d 695, 697 (Fed. Cir. 1985) ("The patentability of a product does not depend on its method of production. If the product in a product-by-process claim is the same as or obvious from a product of the prior art, the claim is unpatentable even though the prior product was made by a different process."). Nevertheless, the Examiner appears to have sought to find in the 8 Appeal2017-006755 Application 12/515,090 art a disclosure of the method of production steps recited in claim 1, likely to help show that other features ( e.g., elements (b) and ( c)) of the claimed pigments are present with the prior art combination. And we are constrained by the Examiner's findings and reasoning on this record. 10 Insofar as the Examiner attempts to find a teaching of the aluminum shot starting material having the specific particle size distribution in part ( 1) of claim 1 's wherein clause (related to the method by which the recited pigments are made), we are unpersuaded such material is disclosed in the cited prior art. Although we agree with the Examiner that Wheeler '079 provides a motivation to use a powder with a narrow particle size distribution for the starting material, Wheeler '079 goes in a different direction than the claims. Wheeler '079 uses a jetting process, not an "atomization of liquid aluminum" as claimed. Wheeler '079, Abstract, ,r,r 1, 18. Moreover, as Appellants note, Wheeler '079 also points out the substantial technical challenges of using an atomization process with aluminum, and further evidences that the result of atomization is conventionally the production of a powder "with a wide particle size distribution." Id. ,r,r 7-9 ("The twin limitations of fine powder production and wide particle size distribution have a consequential limiting effect on the 10 We observe that Schlegl discloses aluminum pigments with a mean thickness range that overlaps with the mean thickness range of claim 1, element (a), and further discloses a L'ih (thickness distribution) that, even if not overlapping, essentially abuts the range recited in element (b) of claim 1. Schlegl, Abstract. Whether element ( c) as recited in claim 1 would be present in such pigments in Schlegl, and whether there is any criticality to a L'ih of 70% and above (as in Schlegl) or less than 70% (as in claim 1) are matters not addressed in the existing appeal record and, thus, are beyond the scope of this decision and appeal. 9 Appeal2017-006755 Application 12/515,090 characteristics of metal flakes prepared from atomised powders."). Even if not a teaching away, as Appellants argue, we are unpersuaded here that the ordinarily skilled person would have had a reasonable expectation of success in providing the aluminum shot material with the specific and narrow particle size distribution recited in step ( 1) of claim 1 's wherein clause. Without a satisfactory showing that the limitations in claim 1 's wherein clause would have been obvious over the cited art, we are unpersuaded the Examiner has demonstrated on this record that the other claim elements - each of limitations (a), (b ), and ( c) are disclosed in the prior art combination. For the above reasons, we are unpersuaded the preponderance of the evidence cited by the Examiner demonstrates that claim 1 ( or the rejected dependent claims) would have been obvious over the applied art. We need not reach Appellants' evidence of alleged unexpected results. Obviousness-Type Double Patenting The Examiner finds that claim 1 would have been obvious over at least claims 6, 7, and 9 of the '832 patent. Non-Final Act. 19. According to the Examiner, the "difference between the instantly rejected claims and the claims of the '832 [patent] is that the claims of the '832 [patent] are drawn to a composition comprising the instantly claimed aluminum pigments." Id. Moreover, the Examiner concludes, claim 1 is merely an "obvious variant of the claims of the '832 [patent] because [it] includes pigments having the same structures and properties as now claimed." Id. at 20. On the issue of obviousness-type double patenting, the Examiner's findings and conclusion are persuasive. Claim 1 of the '832 patent is to a preparation including aluminum effect pigments; dependent claim 6 recites an average pigment thickness from 15 to 150 nm; dependent claim 7 recites that the pigments have a thickness distribution L'ih of 30-150%; and 10 Appeal2017-006755 Application 12/515,090 dependent claim 9 recites an x-ray diffractogram on the pigments showing main peaks that are [111] or [222] reflections. '832 patent, 18:8-17, 18:30- 39, 18:48-52. Hence, the claims of the '832 patent, in combination, disclose each of limitations (a), (b ), and ( c) of pending claim 1. As explained above, the method of production steps in claim 1 's wherein clause are not limiting where, as Appellants urge, the claim is drafted in product-by-process form. In re Thorpe, 777 F .2d at 697. Appellants' only argument related to the double patenting rejection is that Minami, Wheeler '079, and Wheeler, do not teach or suggest the use of aluminum shot with the narrow particle size distribution in forming aluminum pigments. App. Br. 11. Again, the aluminum shot relates to the production steps of claim 1, which are legally irrelevant where the claims of the '83 2 alone disclose pigments with all of features (a), (b ), ( c) of claim 1. For the above reasons, the double-patenting rejection of claim 1 is affirmed. Appellants do not argue dependent claims 2, 3, 5-16, and 36-38 separately, and the double-patenting rejection of those claims is, therefore, also affirmed. SUMMARY We reverse the rejection for obviousness, but affirm the rejection for obviousness-type double patenting. TIME PERIOD FOR RESPONSE No time period for taking any subsequent action in connection with this appeal may be extended under 37 C.F.R. § 1.136(a). AFFIRMED 11 Copy with citationCopy as parenthetical citation