Ex Parte Kononenko et alDownload PDFPatent Trial and Appeal BoardAug 31, 201613167233 (P.T.A.B. Aug. 31, 2016) Copy Citation UNITED STA TES p A TENT AND TRADEMARK OFFICE APPLICATION NO. FILING DATE FIRST NAMED INVENTOR 13/167,233 06/23/2011 Yuriy G. Kononenko 54549 7590 09/02/2016 CARLSON, GASKEY & OLDS/PRATT & WHITNEY 400 West Maple Road Suite 350 Birmingham, MI 48009 UNITED STATES DEPARTMENT OF COMMERCE United States Patent and Trademark Office Address: COMMISSIONER FOR PATENTS P.O. Box 1450 Alexandria, Virginia 22313-1450 www .uspto.gov ATTORNEY DOCKET NO. PA17170A; 67097-1458PUS1 CONFIRMATION NO. 7592 EXAMINER ROE, JESSEE RANDALL ART UNIT PAPER NUMBER 1733 NOTIFICATION DATE DELIVERY MODE 09/02/2016 ELECTRONIC Please find below and/or attached an Office communication concerning this application or proceeding. The time period for reply, if any, is set in the attached communication. Notice of the Office communication was sent electronically on above-indicated "Notification Date" to the following e-mail address( es): ptodocket@cgolaw.com PTOL-90A (Rev. 04/07) UNITED STATES PATENT AND TRADEMARK OFFICE BEFORE THE PATENT TRIAL AND APPEAL BOARD Ex parte YURIY G. KONONENKO, IGOR V. BELOUSOV VADIM IVANOVICH, ANDRII MARYNSKYI, and CARL R. SODERBERG Appeal2015-000208 Application 13/167,233 Technology Center 1700 Before MICHAEL P. COLAIANNI, JAMES C. HOUSEL, and BRIAND. RANGE, Administrative Patent Judges. COLAIANNI, Administrative Patent Judge. DECISION ON APPEAL Appeal2015-000208 Application 13/167,233 Appellants appeal under 35 U.S.C. § 134 the final rejection of claims 16-18 and 20-27. We have jurisdiction over the appeal pursuant to 35 U.S.C. § 6(b). We REVERSE. Appellants' invention is directed to superalloy components having a surface zone that includes an oxygen dopant in an amount sufficient to pin any new grain boundaries in the surface zone that occur under a recrystallization condition of 1080°C/1976°F for 4 hours (Spec. ,-r 4; claim 16). Claim 16 is illustrative: 16. A superalloy article comprising: a nickel-based superalloy body that has a surface zone, the surface zone including oxygen dopant in an amount sufficient to pin any new grain boundaries in the surface zone that occur under a recrystallization condition of 1080°C/197 6°F for 4 hours, the amount of oxygen dopant being insufficient to produce a continuous oxide scale on the surface of the nickel-based superalloy body. Appellants appeal the following rejections: 1. Claims 16-18, and 20-27 are rejected under 35 U.S.C. § 112, i-f 1, as failing to comply with the enablement requirement. 2. Claims 16-18, and 20-27 are rejected under 35 U.S.C. § 112, i-f 2, as failing to particularly point out and distinctly claim the subject matter which the applicant regards as the invention. 2 Appeal2015-000208 Application 13/167,233 3. Claims 16-18, and 20-27 are rejected under 35 U.S.C. § 102(b) as anticipated, or, alternatively, under 35 U.S.C. § 103(a) as obvious over Li et al, Oxidation Behavior of a Single-Crystal Ni-Base Superalloy in Air. I: At 800 and 900°C, Oxidation of Metals, Vol. 59, Nos. 5/6, June 2003. FINDINGS OF FACT & ANALYSIS REJECTION (1): Enablement The Examiner concludes that claim 16 is not enabled because the Specification does not set forth how much oxygen would be sufficient to pin any new grain boundaries in the surface zone that occur under a recrystallization condition of 1080°C/1976°F for 4 hours (Final Act. 3). The Examiner has the initial burden to establish a reasonable basis to question the enablement provided for the claimed invention. In re Wright, 999 F.2d 1557, 1562 (Fed. Cir. 1993) (examiner must provide a reasonable explanation as to why the scope of protection provided by a claim is not adequately enabled by the disclosure). A specification disclosure that contains a teaching of the manner and process of making and using the invention in terms which correspond in scope to those used in describing and defining the subject matter sought to be patented must be taken as in compliance with the enablement requirement unless there is a reason to doubt the objective truth of the statements contained therein which must be relied upon for enabling support. In re Marzocchi, 439 F.2d 220, 223 (CCP A 1971 ). "It is incumbent upon the Patent Office, whenever a rejection on this basis [lack of enablement] is made, to explain why it doubts the truth or accuracy of any statement in a supporting disclosure and to back up 3 Appeal2015-000208 Application 13/167,233 assertions of its own with acceptable evidence or reasoning which is inconsistent with the contested statement. Otherwise, there would be no need for the applicant to go to the trouble and expense of supporting his presumptively accurate disclosure." Id. at 224. The minimal requirement is for the examiner to give reasons explaining the uncertainty of the enablement. In re Bowen, 492 F .2d 859, 862-63 ( CCP A 197 4 ). Enablement requires that the specification teach those in the art to make and use the invention without undue experimentation. In re Wands, 858 F.2d 731, 737 (Fed. Cir. 1988). Whether undue experimentation is needed is not a single, simple factual determination, but rather is a conclusion reached by weighing many factual considerations. Id. In the present case, Appellants argue that the Specification provides ample guidance for determining an oxygen content required to pin grain boundaries without undue experimentation (App. Br. 3). Appellants contend that the defined recrystallization condition provides a means to evaluate whether sufficient oxygen dopant is present in the superalloy article (App. Br. 3). Appellants argue that the Specification describes an example where a treatment is applied to a superalloy to dope oxygen into the alloy and the Specification describes that the treatment can vary depending upon the composition of the superalloy. Id. Appellants contend that even if the experimentation is complex, the experimentation required to make and use the claimed superalloy article is not undue (App. Br. 4). The Examiner analyzed the factors enumerated in Wands, 858 F.2d at 737 (hereinafter the "Wands factors") (Final Act. 2-4). The Examiner's findings with regard to many of these factors merely restate the relevant facts of the present appeal; the analysis does not explain how each factor 4 Appeal2015-000208 Application 13/167,233 weighs in favor of lack of enablement. For example, with regard to the factor "Relative Skill in the Art" the Examiner finds that the skill would include "those in the superalloy making art" (Final Act. 4). The Examiner makes no analysis as to whether the skill level is high or low, or favors enablement or lack thereof. With regard to the predictability of the art factor, the Examiner finds that it "[c]ould be predictable or unpredictable." Id. The Examiner does not make any definitive finding that the superalloy art is unpredictable so that outside the examples or disclosures in the Specification undue experimentation would have been required to enable the scope of the claims. Regarding the quantity of experimentation required factor, the Examiner finds that the experimentation "could be 'undue'" (Final Act. 4). The Examiner finds that the number of variables required to determine the amount of oxygen dopant required to pin the grain boundaries is not enough to create a heightened disclosure requirement but nonetheless finds that one must inquire whether one skilled in the art would be required to conduct undue experimentation due to the breadth of the claims. Id. Thus, the Examiner provides an insufficient analysis of how the various Wands factors weigh in favor of lack of enablement. As part of the lack of enablement analysis, the Examiner finds that Appellants have not disclosed the oxygen content necessary to pin the grain boundaries during recrystallization at 1080°C for 4 hours (Final Act. 3-4). However, the Specification discloses that "[t]he amount of oxygen dopant that is needed to pin grain boundaries is a function of the material composition, treatment temperature to introduce the oxygen and level of mechanical stress at the surface zone 34 ... , which, with the teachings of this disclosure, can all be easily experimentally determined." (Spec. i-f 20). In other words, Appellants 5 Appeal2015-000208 Application 13/167,233 via this disclosure in the Specification indicate that level of skill in the art is such that one of ordinary skill in the art would be able to determine experimentally the amount of oxygen dopant needed to pin the grain boundaries that occur at recrystallization condition of 1080°C for 4 hours. The Examiner's enablement analysis does not provide a reason to doubt the objective truth of the statements contained the Specification regarding the level of skill in the art with regard to what would constitute an enabling disclosure in determining the amount of oxygen dopant to pin grain boundaries at a recrystallization condition of 1080°C for 4 hours. Marzocchi, 439 F.2d 220 at 223. The Examiner has not established that based on a consideration of all the analyzed Wands factors, undue experimentation would be required to make and use the claimed subject matter. On this record, we reverse the Examiner's§ 112, ,-r 1, lack of enablement rejection. REJECTION (2): Indefiniteness The Examiner finds with respect to the recitation in claim 16 that "the amount of oxygen dopant being insufficient to produce a continuous oxide scale on the surface of the superalloy body," this phrase would be a relative phrase dependent upon the superalloy composition (which is not set forth in the claim); the phases present within the superalloy composition; the environment (temperature/pressure) the superalloy is exposed to as well as the amount of time the superalloy is exposed to that environment; and the processing history of the superalloy (Final Act. 5). The Examiner finds that whether or not a nickel-based superalloy is able to form new boundaries would be relative to the amounts of cobalt and chromium (Ans. 14). The 6 Appeal2015-000208 Application 13/167,233 Examiner finds that Appellants would need to specify compositions that would be capable of forming new boundaries. Id. Appellants argue that the Examiner's rejection is based solely on the breadth of the claim, not whether one of ordinary skill in the art would understand what is claimed when the claim is read in light of the Specification (App. Br. 6). The preponderance of the evidence favors Appellants' argument of compliance with§ 112, i-f 2. The Examiner's analysis focuses solely on the breadth of the claim encompassing many different superalloy compositions. Breadth, however, is not indefiniteness. In re Miller, 441F.2d689, 693 (CCP A 1971 ). In the present case, when the claim is read in light of the Specification it is clear that the amount of oxygen dopant present in the superalloy is enough to pin grain boundaries at recrystallization condition of 1080°C for 4 hours but the oxygen dopant amount is insufficient to produce a continuous oxide scale on the surface of the superalloy body. There may be many different superalloy compositions that would meet those limitations, but that does not make the claim indefinite. On this record, we reverse the Examiner's § 112, i-f 2, rejection. REJECTION (3): §§ 102(b)/103(a) The Examiner finds that Li teaches a superalloy article that is experimentally processed at a temperature of 800 to 900°C for up to 1925 hours (Final Act. 6). The Examiner finds that since Li discloses the same composition and the same processing or substantially similar processing, a superalloy body having a surface zone including oxygen in an amount sufficient to pin any new grain boundaries in the surface zone that occurs 7 Appeal2015-000208 Application 13/167,233 under a recrystallization condition of 1080°C/197 6°F for 4 hours would be expected (Final Act. 6). Alternatively, the Examiner concludes that it would have been obvious to one having ordinary skill in the art at the time the invention was made to select the temperature and time of treatment, as set forth in [0023] of the instant Specification, from that disclosed by Li because Li discloses the same utility (oxidation behavior of single crystal nickel base superalloys) (Final Act. 6-7). The Examiner further finds that with respect to the added recitation "the amount of oxygen dopant being insufficient to produce a continuous oxide scale on the surface of the superalloy body" in claim 16, Li teaches that at 800 °C the superalloy exhibited non-uniform oxidation or highly non-uniform oxidation (non-continuous) (abstract and conclusions). However, a continuous oxide scale is not disclosed or suggested and, therefore, Li meets the claim. (Final Act. 7). Appellants argue that Li fails to characterize the resulting oxidation on the superalloy as discontinuous as the Examiner finds (App. Br. 7). Appellants contend that Li's disclosure analyzes the different oxide morphologies that form on the superalloy and do not indicate that the oxide is discontinuous. Id. Appellants argue that the Examiner's presumption of an identical product resulting from the same alloy being processed in the same manner described in the Specification is unnecessary because Li discloses that a continuous, multilayer oxide film forms on the alloy after the treatment (Reply Br. 4-5). The preponderance of the evidence favors Appellants' argument of novelty and nonobviousness. With regard to the anticipation rejection, the Examiner has not established that Li teaches a superalloy made in the same manner as described in the Specification. Particularly, the Specification 8 Appeal2015-000208 Application 13/167,233 describes that an oxygen doping treatment includes heating between 800 and 900°C for 2 hours in air (Spec. ,-r 23). The Specification describes that Figures 5 and 6 show the effect of vacuum annealing (i.e., no air for oxygen doping) for 3 hours at a temperature of 870 to 1040°C after which time a recrystallization condition of 1080°C for 4 hours was applied (Spec. i-f 25). Figure 6 shows that a recrystallization layer 40 forms. Id. Li discloses heating the superalloy at a temperature of 800 to 900°C for up to 1925 hours (Li 592 "Experimental Procedures"). Li exemplifies using a minimum treatment time of 5 hours with a continuous oxide scale forming on the superalloy (Li 596 Table I; Fig. 3). Li's Figure 3A shows dendrite and interdendrite formations with an oxide scale formed across the entire superalloy surface treated for 5 hours at 800°C (Li 596-597, "Scale Morphologies and Composition at 800°C"). Accordingly, Li does not disclose within the meaning of35 U.S.C. § 102 the subject matter of claim 1. With regard to the obviousness rejection, the Examiner finds that Li discloses treating a superalloy at a temperature of 800 to 900°C for up to 1925 hours. In other words, it appears that Li's treatment time overlaps with the described treatment time of 2 hours at a temperature of 800 to 900°C. Ans. 16. Li further describes, however, the shortest treatment time as being 5 hours with longer treatment times taught (Li 596 Table 1 ). Li discloses that an oxide layer is formed on the surface of the superalloy in dendritic (i.e., area A in Figure 3a) and interdendritic areas (i.e., area B in Figure 3a) on a superalloy surface treated for 5 hours at 800°C. The interdendritic areas are areas between the raised dendritic areas in Figure 3a. Li appears to 9 Appeal2015-000208 Application 13/167,233 disclose that the oxide formation is continuous over the portion of the article shown in Figure 3b. The Examiner focuses on Li's overlapping range of treatment time (i.e., up to 1925 hours) with the time range disclosed by Appellants (i.e., 2 hours) at a temperature of 800°C (Ans. 16-17). Li teaches, however, using treatment times longer than 2 hours (i.e., 5 hour minimum treatment time is disclosed). In other words, Li would have led the ordinarily skilled artisan away from the treatment times exemplified by Appellants. Accordingly, the Examiner has not established that Li would have suggested using Appellants' 2 hour treatment time at 800°C with Li's superalloy treatment. On this record, we reverse the Examiner's §102(b) and§ 103(a) rejection over Li. DECISION The Examiner's decision is reversed. ORDER REVERSED 10 Copy with citationCopy as parenthetical citation