Ex Parte HelbergDownload PDFPatent Trial and Appeal BoardAug 21, 201813980580 (P.T.A.B. Aug. 21, 2018) Copy Citation UNITED STA TES p A TENT AND TRADEMARK OFFICE APPLICATION NO. FILING DATE 13/980,580 07/19/2013 129406 7590 The Chemours Company Patent Legal Group 1007 Market Street 8072 Wilmington, DE 19801 08/23/2018 FIRST NAMED INVENTOR Lisa Edith Helberg UNITED STATES DEPARTMENT OF COMMERCE United States Patent and Trademark Office Address: COMMISSIONER FOR PATENTS P.O. Box 1450 Alexandria, Virginia 22313-1450 www .uspto.gov ATTORNEY DOCKET NO. CONFIRMATION NO. TT0126USPCT 6540 EXAMINER DOYLE, BRANDI M ART UNIT PAPER NUMBER 1771 NOTIFICATION DATE DELIVERY MODE 08/23/2018 ELECTRONIC Please find below and/or attached an Office communication concerning this application or proceeding. The time period for reply, if any, is set in the attached communication. Notice of the Office communication was sent electronically on above-indicated "Notification Date" to the following e-mail address(es): patentlegal@chemours.com gwen.a.wilson@chemours.com PTOL-90A (Rev. 04/07) UNITED STATES PATENT AND TRADEMARK OFFICE BEFORE THE PATENT TRIAL AND APPEAL BOARD Ex parte LISA EDITH HELBERG Appeal2017-009950 Application 13/980,580 Technology Center 1700 Before TERRY J. OWENS, LINDA M. GAUDETTE, and DONNA M. PRAISS, Administrative Patent Judges. PRAISS, Administrative Patent Judge. DECISION ON APPEAL 1 STATEMENT OF THE CASE This is an appeal under 35 U.S.C. § 134(a) from the final rejection of claims 1-3, 5-11, and 13-16. We have jurisdiction under 35 U.S.C. § 6. We AFFIRM. The subject matter of this appeal relates to "a process for purifying TiCl4 produced via a chloride process" which is a critical step in titanium metal manufacture. Spec. 1:9-10, 1 :22-24. More specifically, tin metal or 1 This decision makes reference to the Specification filed July 19, 2013 ("Spec."), the Final Office Action dated July 14, 2016 ("Final Act."), the Appeal Brief filed January 10, 2017 ("Br."), and the Examiner's Answer dated May 19, 2017 ("Ans."). Appeal2017-009950 Application 13/980,580 SnCb is used to remove vanadium from crude TiC14 produced via the chloride process. Id. 3:13-15. Claim 1 is illustrative (disputed elements italicized): 1. A process for the purification of TiC 14 comprising the steps of: (a) contacting vanadium-containing crude TiC1 4 with tin to produce purified TiCl4, SnCl4, and solid vanadium; and (b) separating the solid vanadium from the purified TiCl4 and SnCl4; wherein the contacting and separating steps are performed by a two stage process comprising: (i) reducing the vanadium content in the vanadium- containing crude TiC1 4 by contacting the vanadium- containing crude TiC1 4 with a less than excess amount of tin to produce partially purified TiCl4, SnCl4, and solid vanadium; (ii) separating the solid vanadium from the partially purified TiCl4 and SnCl4; (iii) further reducing the vanadium content in the partially purified TiCJ 4 by contacting the partially purified TiCJ 4 with an excess of tin to produce purified TiCJ4, SnCJ4, solid vanadium, and excess tin; and (iv) separating the solid vanadium and excess tin from the purified TiCl4 and SnCk Br., Appendix 1, 1. Independent claim 9, the only other independent claim in this appeal, differs from claim 1 in that claim 9 recites "SnCb" instead of "tin." Id. at 2. The Examiner maintains, and Appellant2 appeals, the following rejections under 35 U.S.C. § 103: 2 The Chemours Company TT, LLC is identified as the real party in interest. Br. 3. 2 Appeal2017-009950 Application 13/980,580 1. Claims 1, 5, and 8 over Hansley; 3 2. Claims 9, 13, and 16 over Hansley in view ofHudlicky; 4 3. Claims 2, 3, 10, and 11 over Hudlicky and/or Hansley as applied to claims 1 and 9 in Rejections 1 and 2, further in view of Stoddard5 and Fahnoe· 6 ' 4. Claims 6 and 14 over Hudlicky and/or Hansley as applied to claims 5 and 13 in Rejections 1 and 2, further in view of Pefferman7; and 5. Claims 7 and 15 over Hudlicky and/or Hansley as applied to claims 1 and 9 in Rejections 1 and 2, further in view of Stoddard. Ans. 2; Br. 8-11. OPINION After review of the arguments and evidence presented by both Appellant and the Examiner, we affirm the stated rejections for the reasons provided in the Final Office Action and the Answer. We add the following primarily for emphasis. Rejection 1 It is the Examiner's position that claims 1, 5, and 8 are unpatentable as obvious over Hansley for the reasons stated on pages 3--4 of the Final Office Action. 3 Hansley et al., US 2,958,574, issued Nov. 1, 1960 ("Hansley"). 4 MILOS HUDLICKY, REDUCTIONS IN ORGANIC CHEMISTRY, pp. 29-30, 214 (1984) ("Hudlicky"). 5 Stoddard et al., US 2,836,547, issued May 27, 1958 ("Stoddard"). 6 Fahnoe et al., US 3,156,630, issued Nov. 10, 1964 ("Fahnoe"). 7 Pefferman, US 3,744,978, issued July 10, 1973 ("Pefferman"). 3 Appeal2017-009950 Application 13/980,580 In the Appeal Brief, Appellant argues the subject matter of claims 1, 5, and 8 as a group. In accordance with 37 C.F.R. § 4I.37(c)(l)(iv), claims 5 and 8 will stand or fall together with claim 1, which is representative of the group. Appellant contends that the rejection is in error because Hansley discloses the use of finely divided metals to produce a purified TiC14, therefore one skilled in the art would "believe that no further purification is necessary" and "would not be motivated to split the contacting and separation step from the process of Hansley into two duplicate steps." Br. 8-9. Appellant asserts that the vanadium concentration is only partially reduced in claim 1 so that the tin metal reaction can be driven to completion. Id. at 9 ( citing Spec. 7: 13-17). Appellant contends that "the claimed invention results in improved kinetics not disclosed or suggested by [Hansley]." Id. The Examiner responds that Hansley uses the same reactants and reaction mechanism as Appellant to achieve the same result and that the steps of claim 1 "merely duplicat[ e] the known process steps of Hansley and combine[e] these known steps in a known way." Ans. 9. Regarding Appellant's assertion that the claimed steps result in improved kinetics, the Examiner finds that neither Appellant's Specification nor Appellant's Appeal Brief suggests any unexpected results from modifying the known TiC14 purification process to be performed in two stages rather than one. Id. at 10. We are not persuaded of reversible error in the Examiner's rejection of claim 1 based on the cited record in this appeal. 4 Appeal2017-009950 Application 13/980,580 Appellant does not dispute the Examiner's finding (Ans. 9) that Hansley teaches the same reactants, the same reaction mechanism, and the same results of claim 1 and differs only in the number of stages used. Instead, Appellant contends (Br. 9) that improved kinetics result from partially reducing the vanadium concentration in the first stage in order to drive the tin metal reaction to completion. Appellant, however, does not direct us to any evidence that the alleged improvement produces different results over a one stage process or otherwise would not have been expected from performing Hansley's process in two stages. See In re Harza, 274 F.2d 669, 671 (CCPA 1960) (noting that merely duplicating parts has no patentable significance unless a new and unexpected result is produced). Appellant's Specification discloses that the purification reaction can be performed in either a single stage or two stage configuration, with the benefit of the two stage configuration being less excess tin is used. Spec. 5:18-22. This disclosure further supports the Examiner's finding that Appellant's method would have been expected to produce the same results as Hansley's method. Accordingly, in the absence of any evidence of a new and unexpected result, we find the preponderance of the evidence in this record supports the stated rejection of claim 1 as well as claims 5 and 8 under 35 U.S.C. § 103. Rejection 2 It is the Examiner's position that claims 9, 13, and 16 are unpatentable as obvious over Hansley in view of Hudlicky for the reasons stated on pages 4--5 of the Final Action. 5 Appeal2017-009950 Application 13/980,580 In the Appeal Brief, Appellant argues the subject matter of claims 9, 13, and 16 as a group. In accordance with 37 C.F.R. § 4I.37(c)(l)(iv), claims 13 and 16 will stand or fall together with claim 9, which is representative of the group. Appellant contends that the rejection is in error because tin and SnCh are not functionally equivalent on the basis that stannous chloride is not as efficient as tin. Br. 10. Appellant asserts that the cited prior art would not motivate one skilled in the art to modify the teachings of Hansley when Hansley teaches away from using certain metal powders and tin is more efficient than SnCh. Id. at 10-11. The Examiner responds that the substitution of one known element for another to obtain predictable results does not require the substitutable elements achieve the exact same results. Ans. 10. The Examiner further finds that Hudlicky teaches that stannous chloride provides other benefits over tin such as solubility and reduced cost, thus, even if stannous chloride is not as efficient as tin in its metal form, "[b ]oth Sn Ch and Sn are known reducing agents which may be used to react with and remove the vanadium impurities in the TiCl4 purification process." Id. Appellant's argument distinguishing SnCh and Sn on the basis that the known reducing agents have different efficiencies is not persuasive of error by the Examiner. The Examiner's finding that both Sn Ch and Sn are known reducing agents and interchangeable in reduction reactions is supported by the record. Hudlicky at 30. The record also supports the Examiner's finding that both SnCh and Sn have benefits associated with their use. Id. Therefore, the substitution of SnCh for Sn would have been motivated by the benefits associated with SnCh. See In re Urbanski, 809 6 Appeal2017-009950 Application 13/980,580 F.3d 1243 (Fed. Cir. 2016) ("[T]he Board properly found that one of ordinary skill would have been motivated to pursue the desirable properties taught by Wong, even at the expense of foregoing the benefit taught by Gross."). Because we are not persuaded of error in the Examiner's rejection of claim 9 over the combination of Hansley and Hudlicky, we also affirm the Examiner's decision to reject claims 13 and 16 as well. Re} ections 3-5 It is the Examiner's position that claims 2, 3, 6, 7, 10, 11, 14, and 15 are unpatentable as obvious over Hudlicky and/or Hansley in combination with various secondary references for the reasons stated on pages 5-7 of the Final Action. In the Appeal Brief, Appellant argues that the Examiner erred for the same reasons claims 1 and 9 are distinguishable over the cited art and that the additional cited prior art references do not remedy the asserted deficiencies of Hansley and Hudlicky. Br. 11. Appellant's assertion is insufficient to state a separate argument for claims 2, 3, 6, 7, 10, 11, 14, and 15. In re Lovin, 652 F.3d 1349, 1357 (Fed. Cir. 2011 ). Because we are not persuaded of error in the Examiner's rejection of claims 1 and 9 for the reasons discussed above, we likewise affirm the Examiner's decision to reject claims 2, 3, 6, 7, 10, 11, 14, and 15 under 35 U.S.C. § 103. 7 Appeal2017-009950 Application 13/980,580 DECISION For the foregoing reasons, we affirm all of the Examiner's rejections under 35 U.S.C. § 103. No time period for taking any subsequent action in connection with this appeal maybe extended under 37 C.F.R. § 1.136(a)(l). AFFIRMED 8 Copy with citationCopy as parenthetical citation