Ex Parte Haas et alDownload PDFPatent Trials and Appeals BoardMay 15, 201913518435 - (D) (P.T.A.B. May. 15, 2019) Copy Citation United States Patent and Trademark Office UNITED STATES DEPARTMENT OF COMMERCE United States Patent and Trademark Office Address: COMMISSIONER FOR PATENTS P.O.Box 1450 Alexandria, Virginia 22313-1450 www.uspto.gov APPLICATION NO. FILING DATE FIRST NAMED INVENTOR ATTORNEY DOCKET NO. CONFIRMATION NO. 13/518,435 09/26/2012 Herwig Haas 3926.367 2613 41288 7590 05/15/2019 PATFNT TFNTR AT T T C EXAMINER Stephan A. Pendorf DOVE, TRACY MAE 1401 Hollywood Boulevard Hollywood, EL 33020 ART UNIT PAPER NUMBER 1727 MAIL DATE DELIVERY MODE 05/15/2019 PAPER Please find below and/or attached an Office communication concerning this application or proceeding. The time period for reply, if any, is set in the attached communication. PTOL-90A (Rev. 04/07) UNITED STATES PATENT AND TRADEMARK OFFICE BEFORE THE PATENT TRIAL AND APPEAL BOARD Ex parte HERWIG HAAS, JOY ROBERTS, FRANCINE BERRETTA, AMY SHUN-WEN YANG, YVONNE HSIEH, GUY PEPIN, ANDREW LEOW, RICHARD FELLOWS, and NICOLAE BARS AN Appeal 2018-006119 Application 13/518,435 Technology Center 1700 Before LINDA M. GAUDETTE, CHRISTOPHER C. KENNEDY, and JANE E. INGLESE, Administrative Patent Judges. GAUDETTE, Administrative Patent Judge. DECISION ON APPEAL1 The Appellants2 appeal under 35 U.S.C. § 134(a) from the Examiner’s decision finally rejecting claims 30—38, 43—45, and 59 under (1) 35 U.S.C. § 112(a)or35U.S.C. § 112 (pre-AIA), first paragraph, as failing to comply with 1 This Decision includes citations to the following documents: Specification filed June 22, 2012 (“Spec.”); Final Office Action dated June 13, 2017 (“Final”); Appeal Brief filed Jan. 16, 2018 (“Appeal Br.”); Examiner’s Answer dated Mar. 22, 2018 (“Ans.”); and Reply Brief filed May 22, 2018 (“Reply Br.”). 2 The Appellants identify the real parties in interest as Daimler AG of Stuttgart, Germany, and Ford Motor Company of Dearborn, Michigan. Appeal Br. 3. Appeal 2018-006119 Application 13/518,435 the written description requirement; and (2) 35 U.S.C. § 102(b) as anticipated by (a) Lee,3 (b) Ye,4 and (c) Hill.5’6 We AFFIRM. The invention relates to a solid polymer electrolyte fuel cell. Spec. 1. A solid polymer electrolyte fuel cell stack for generating electricity at useful voltages generally includes several to many unit cells stacked in multi-layers, each unit cell being formed with a membrane-electrode assembly (MEA) comprising an anode, a cathode, and a solid polymer electrolyte membrane therebetween. Id. at 5. Both the anode and the cathode comprise catalysts (e.g. platinum). Id. MEAs often include porous, electrically conductive, gas diffusion layers (GDLs) adjacent the anode (oxidation electrode) and cathode (reduction electrode) for purposes of distributing reactants to and by-products from these electrodes. Id. Electrically conductive flow field plates comprising a plurality of channels patterned therein are employed to evenly distribute reactants to, and by-products from, the adjacent GDLs. Id. “Hydrogen fuel is supplied to the anode and adsorbed on the anode catalyst, often present in the form of a catalyst coating on the membrane electrolyte . . . . The fuel is oxidized to produce protons and electrons.” Id. “The electrons are transferred to the cathode via an external circuit, and the protons are transferred to the cathode through the polymer electrolyte membrane.” Id. The protons, electrons, and an oxidant, typically air, are reacted on the catalyst present on or in the cathode to product electricity and water. Id. 3 US 2006/0134501 Al, pub. June 22, 2006. 4 WO 2008/024465 A2, pub. Feb. 28, 2008. 5 GB 2,309,230 A, pub. July 23, 1997. 6 We have jurisdiction under 35 U.S.C. § 6(b). 2 Appeal 2018-006119 Application 13/518,435 According to the Specification, “[d]uring the start-up and shut-down of fuel cell systems, corrosion enhancing events can occur.” Id. at 1. “In particular, air can be present at the anode . . . and the transition between air and fuel in the anode is known to cause temporary high potentials at the cathode, thereby resulting in carbon corrosion and platinum catalyst dissolution, . . . [and] significant performance degradation over time.” Id. The inventive solid polymer electrolyte fuel cell incorporates a selectively conductive component that is said to prevent temporary high cathode potentials during fuel cell start-up and shut-down. Id. at 2. Of the appealed claims, claim 30, reproduced below, is the sole independent claim. See generally Appeal Br. 24—26 (Claims Appendix) 30. A solid polymer electrolyte fuel cell, the fuel cell comprising a solid polymer electrolyte, cathode components, and anode components connected in series electrically, wherein: the cathode components comprise a cathode electrode, a cathode gas diffusion layer, and a cathode fuel flow plate; the anode components comprise an anode electrode, an anode gas diffusion layer, and an anode fuel flow plate; and a selectively conducting material is provided in at least one of the anode components in an amount sufficient to render the electrical resistance of the anode component containing the selectively conducting material in the presence of air is greater than 10'3 ohm over 1 square meter area and in the presence of hydrogen is more than 100 times lower than the electrical resistance of the anode component containing the selectively conducting material in the presence of air. Id. at 24. Rejection under 35 U.S.C. § 112, written description requirement Claim 30 recites “the electrical resistance of the anode component containing the selectively conducting material in the presence of air is greater than 10'3 ohm over 1 square meter area.” The Examiner found the written description discloses that the selectively conducting material may have an electrical resistance 3 Appeal 2018-006119 Application 13/518,435 in air of greater than 10'3 ohm over 1 square meter. Final 2—3 (citing Spec. 9—10). The Examiner found no support, however, for an anode component having this electrical resistance. Id. at 3. The Examiner thus determined the claims fail to comply with the written description requirement of 35 U.S.C. § 112 .Id. at 2. In the Answer, the Examiner clarifies that the written description describes only the selectively conducting material or layer, but not the anode component containing the selectively conducting material or layer, as having an electrical resistance in air of greater than 10'3 ohm over 1 square meter. Ans. 6. The Appellants argue it is not the selectively conducting material, but “the ‘anode component containing the selectively conducting material’ that must be formulated to have the selectively conducting properties.” Appeal Br. 8. The Appellants contend “[t]he ‘component’ may be a solid coating, or it may be embodied in the anode or the anode gas diffusion layer (GDL).” Id. (emphasis omitted). As further discussed below, the Appellants misapprehend the Examiner’s position, and their arguments are not persuasive of reversible error in the Examiner’s rejection of claims 30-38, 43—45, and 59 under 35 U.S.C. § 112(a) or 35 U.S.C. § 112 (pre-AIA), first paragraph, as failing to comply with the written description requirement. The Specification discloses that the selectively conducting component may comprise a layer of the selectively conducting material, and that the layer can be incorporated in numerous ways within the anode components of the fuel cell. Spec. 3. “For instance, the layer may be part of the anode and thus the selectively conducting component is the anode itself.'’'’ Id. (emphasis added). The Specification discloses that “the selectively conducting component may be the anode flow field plate itself with the layer of the selectively conducting material incorporated on the 4 Appeal 2018-006119 Application 13/518,435 side of the anode flow field plate adjacent the anode gas diffusion layer. Id. at 4. The Specification also discloses that it is “possible to employ a discrete selectively conducting layer within the series connected anode components. In such a case, the selectively conducting component is the discrete selectively conducting layer.'1'’ Id. (emphasis added). From this disclosure, one of ordinary skill in the art would understand that the selectively conducting component may be a component made up in part, or in its entirety, of a layer of the selectively conducting material. Thus, we disagree with the Appellants that the selectively conducting component may be a coating. Rather, in the case of a GDL coated with a selectively conducting material, for example, one of ordinary skill in the art would understand from the Specification that the selectively conducting component is the GDL plus the coating. See, e.g., Spec. 12 (describing preparation of selectively conducting GDL components by coating selectively conducting layers onto test GDL samples). Turning to the claims, we note that claim 45, which depends from claim 30, recites that the selectively conducting material is provided on a side of the anode GDL, on a side of the anode flow field plate, or as a separate discrete layer. Therefore, the broadest reasonable construction of the claim 30 recitation “a selectively conducting material is provided in at least one of the anode components” encompasses embodiments wherein the selectively conducting component is made up of a layer of the selectively conducting material either in part (i.e., a layer on the side of the GDL or anode flow field plate) or in its entirety (i.e., a separate discrete layer). From the Specification disclosure cited in the paragraph below, however, we find the written description supports the claim 30 recitation requiring that “the electrical resistance of the anode component containing the selectively conducting material in the presence of air is greater than 10'3 ohm over 1 square meter area” (emphasis added), only in the case where the 5 Appeal 2018-006119 Application 13/518,435 selectively conducting layer makes up the entirety of the selectively conducting component. The Specification discloses that “[t]he properties of the selectively conducting layer, regardless of where and in what form it appears, need to be tailored to certain specific system needs. . . . [T]he layer has to be engineered . . . such that it has acceptable conductance in the presence of hydrogen and yet is sufficiently resistive in the presence of oxygen (air).” Spec. 9 (emphasis added). “The layer must have sufficient resistance to prevent local high voltages and reduce corrosion currents in practice during the startup and shutdown transitions.” Id. According to the Specification, “[f]or certain commercial applications, modelling suggests for instance that good resistance targets may involve a three order of magnitude change in resistance, such as over 10'3 ohms/m2 in air and less than 10'6 ohms/m2 in hydrogen.” Id. The Specification describes preparation of selectively conducting components by coating solid-liquid dispersions of metal oxide compositions onto GDL samples. Id. at 12. To obtain “information on the actual resistance characteristics expected of the selectively conducting layer on these GDLs,” resistance measurements were made on several related samples in a closed, environmentally controlled chamber. Id. at 14 (emphasis added). In sum, based on our review of the claim language in light of the Specification, we determine the written description fails to support the entire genus of anode components containing a selectively conducting material that is encompassed by claim 30. We sustain the rejection of claims 30—38, 43—45, and 59 under 35U.S.C. § 112(a)or35U.S.C. § 112 (pre-AIA), first paragraph, as failing to comply with the written description requirement. 6 Appeal 2018-006119 Application 13/518,435 Rejections under 35 U.S.C. § 102(b) The Examiner’s rejections under 35 U.S.C. § 102(b) are based on a finding that each of the cited references (Lee, Ye, or Hill), uses a metal oxide (i.e., a selectively conducting material as claimed) as a coating layer, and, therefore, the anode components containing the metal oxide in each of the references inherently possesses the claimed electrical resistance characteristics. See Final 3^4; Ans. 10— 12. To establish inherency, the extrinsic evidence must make clear that the missing descriptive matter is necessarily present in the thing described in the reference. In re Robertson, 169 F.3d 743, 745 (Fed. Cir. 1999). Inherency, however, may not be established by probabilities or possibilities. Id. The mere fact that a certain thing may result from a given set of circumstances is not sufficient. Id. The Appellants argue that the “[m]ere presence of metal oxide does not impart selective conductivity.” Appeal Br. 13. The Appellants direct us to the disclosure at pages 9—10 of the Specification (Appeal Br. 9), which supports this argument: Because the change in resistance with surrounding atmosphere is associated with changes at the surface of the metal oxide particles as opposed to the bulk, the choice of metal oxide material, its particle size and shape, the thickness and porosity of the fabricated layer, along with other variables are all important considerations. (Spec. 9). “Layer thicknesses may for instance be expected in the range from about 1 pm to 300 pm. And particle sizes may be in the range of 10—25 nm with surface areas of 40 m2/g to 200 m2/g.” Id. The Appellants argue the applied prior art does not distinguish between use of the coating materials used at the anode or cathode. Appeal Br. 16. The Appellants contend, therefore, that the prior art coating materials cannot have the same electrical resistance characteristics as claimed 7 Appeal 2018-006119 Application 13/518,435 because the resistance would be unacceptably high in the presence of air and the prior art fuel cells would not work properly when the coating was used on the cathode side where the selectively conducting component would always be in air. Id. The Appellants have argued persuasively that the Examiner has failed to provide sufficient evidence to support a finding that the claimed electrical resistance characteristics are necessarily present in the prior art coatings. Accordingly, we do not sustain the rejections of claims 30-38, 43—45, and 59 under 35 U.S.C. § 102(b) as anticipated by (a) Lee, (b) Ye, and (c) Hill. ORDER We affirm the rejection of claims 30-38, 43—45, and 59 under 35 U.S.C. § 112(a)or35U.S.C. § 112 (pre-AIA), first paragraph, as failing to comply with the written description requirement. We reverse the rejections of claims 30-38, 43—45, and 59 under 35 U.S.C. § 102(b). No time period for taking any subsequent action in connection with this appeal may be extended under 37 C.F.R. §1.136(a)(l)(iv). AFFIRMED 8 Copy with citationCopy as parenthetical citation