Ex Parte Gross et alDownload PDFPatent Trial and Appeal BoardSep 27, 201612359662 (P.T.A.B. Sep. 27, 2016) Copy Citation UNITED STA TES p A TENT AND TRADEMARK OFFICE APPLICATION NO. FILING DATE 12/359,662 01/26/2009 60476 7590 09/29/2016 PA TENT DOCKET DEPARTMENT ARMSTRONG TEASDALE LLP 7700 Forsyth Boulevard Suite 1800 St. Louis, MO 63105 FIRST NAMED INVENTOR Adam Franklin Gross UNITED STATES DEPARTMENT OF COMMERCE United States Patent and Trademark Office Address: COMMISSIONER FOR PATENTS P.O. Box 1450 Alexandria, Virginia 22313-1450 www .uspto.gov ATTORNEY DOCKET NO. 08-0913-US-NP (24691-248) CONFIRMATION NO. 4838 EXAMINER GAITONDE, MEG HA MEHTA ART UNIT PAPER NUMBER 1781 NOTIFICATION DATE DELIVERY MODE 09/29/2016 ELECTRONIC Please find below and/or attached an Office communication concerning this application or proceeding. The time period for reply, if any, is set in the attached communication. Notice of the Office communication was sent electronically on above-indicated "Notification Date" to the following e-mail address( es): USpatents@armstrongteasdale.com patentadmin@boeing.com PTOL-90A (Rev. 04/07) UNITED STATES PATENT AND TRADEMARK OFFICE BEFORE THE PATENT TRIAL AND APPEAL BOARD Ex parte ADAM FRANKLIN GROSS and WILLIAM B. CARTER Appeal2015-002523 Application 12/359,662 Technology Center 1700 Before KAREN M. HASTINGS, A VEL YN M. ROSS, and JENNIFER R. GUPTA, Administrative Patent Judges. GUPTA, Administrative Patent Judge. DECISION ON APPEAL Appellants 1 appeal under 35 U.S.C. § 134(a) from the Examiner's decision2 finally rejecting claims 1-12. We have jurisdiction under 35 U.S.C. § 6(b). We affirm. The claims are directed to a method for bonding nano-elements to a surface. Spec. i-f 6. Claim 1, reproduced below, is illustrative of the claims on appeal. 1 Appellants identify the real party in interest as The Boeing Company. Appeal Brief filed September 5, 2014 ("App. Br."), 1. 2 Final Office Action mailed June 5, 2014 ("Final Act."). Appeal2015-002523 Application 12/359,662 1. A method for bonding nano-elements to a surface, said method comprising: applying layers of metal onto a top of a nano-element array of a plurality of substantially aligned nano-elements, the layers of metal including a substantially continuous layer of an inert metal bonded to tips of the plurality of aligned nano-elements, wherein at least a portion of said substantially continuous layer infiltrates at least a portion of the nano-element array, and a first layer of a first active metal applied onto the layer of the inert metal; positioning a layer of a second active metal adjacent to the first layer of the first active metal; placing a compressive force of less than about 6.1 psi across the nano-elements, the metal layers, and a substrate adjacent the second layer of a second active metal to facilitate forming at least one of a eutectic bond, a metal solid solution, and an alloy bond between the nano-elements and the substrate; and elevating the temperature of the nano-elements, the metal layers, and the substrate such that the first and second active metals form at least one of the eutectic bond, the metal solid solution, and the alloy bond between the nano-elements and the substrate. App. Br. (Claims Appendix) 10. DISCUSSION Claims 1-12 stand rejected under 35 U.S.C. § 103(a) as unpatentable over Zhang et al. (US 2004/0266065 Al, published Dec. 30, 2004) (hereinafter "Zhang") in view of Stacey (US 5,021,300, issued Jun. 4, 1991) (hereinafter "Stacey") and Ouellet et al. (US 2004/0067604 Al, published Apr. 8, 2004) (hereinafter "Ouellet"), and further in view of Graham, Jr. et al. (US 2009/0246507 Al, published Oct. 1, 2009) (hereinafter "Graham"). Final Act. 2---6. 2 Appeal2015-002523 Application 12/359,662 Appellants argue the claims as a group. See generally App. Br. 3-8. We select claim 1 as representative of the rejected claims, and the remaining claims on appeal will stand or fall with claim 1. See 37 C.F.R. § 41.37 ( c )(1 )(iv) (2015). The Examiner finds that Zhang teaches a method for making a carbon nanotube device that includes growing carbon nanotubes on a substrate 310 (Zhang i-f 24), and then depositing a layer of metal 330, which may comprise copper (inert material) over the carbon nanotube array 320 and substrate 310 to form a metal matrix around the carbon nanotubes 325 (Id. i-f 25; Figs. 3A, 3B). Ans. 2-3. The Examiner also finds that Zhang teaches that the metal layer 330 extends above the upper ends (tips) of the nanotubes 325 (Zhang i-f 30; Fig. 3B). See id. The Examiner finds that Zhang teaches a solder metal layer 340 (first layer of a first active metal) may be deposited over the layer of metal 330 (Zhang i-f 29; Fig. 3D). Final Act. 2. However, the Examiner acknowledges that Zhang does not teach a layer of a second active metal adjacent to the first layer of the first active metal or placing a compressive force of less than about 6.1 psi across the nano-elements, the metal layers, and substrate and elevating the temperature of the nano- elements, the metal layers, and the substrate to form a eutectic bond between the nano-elements and the substrate. Id. The Examiner finds, and Appellants do not dispute, that Stacey teaches a method for forming a solder bond for use in bonding electrical components to substrates that includes depositing a first active metal layer comprising copper or gold over a substantially continuous layer of an inert metal, and depositing a second active metal layer comprising tin or cadmium over the first active metal layer (Stacey 3:60-66), and heating the layers to 3 Appeal2015-002523 Application 12/359,662 form a eutectic bond that firmly bonds the structure together (Id. at 4:50-66; Abstract). Final Act. 2-3. The Examiner finds, and Appellants do not dispute, that one of ordinary skill in the art would have been motivated, based on Stacey, to use a solder back that includes two alloy component layers as Zhang's solder layer to form a eutectic bond that firmly bonds the layers of Zhang's carbon nanotube structure together even at elevated temperatures. Id. The Examiner finds that neither Zhang nor Stacey teach applying pressure to the nano-elements, the metal layers, and the substrate to form a eutectic bond. Id. at 3. The Examiner, however, finds, and Appellants do not dispute, that Ouellet teaches a method for manufacturing an integrated device (Ouellet i-f 3; 5) including a cadmium gold solder bond between two wafers, and applying compressive force across the components and elevating the temperature of the components such that the metal layers form a eutectic bond (Id. at i-fi-1145, 149). Final Act. 3. The Examiner finds, and Appellants do not dispute, that one of ordinary skill in the art would have been motivated, based on Ouellet, to apply pressure to bond Zhang's nano- elements and metal layers to form a strong eutectic bond, without voids, between the layers. See id. at 3. The Examiner acknowledges that Ouellet does not disclose the claimed range of pressure, but finds that Graham teaches bonding carbon nanotubes to a silicon substrate with a combination of gold, indium, and tin layers using a pressure of less than 30 psi (Graham i-f 37). Final Act. 3--4. The Examiner finds, and Appellants do not dispute, that one of ordinary skill in the art would have been motivated, based on Graham, to apply low pressure to Zhang's carbon nanotube structure 4 Appeal2015-002523 Application 12/359,662 because one of ordinary skill in the art would appreciate that low pressure is required to avoid crushing the carbon nanotube device. Id. at 4. Appellants argue the Examiner reversibly erred in finding that Zhang alone or in combination with Stacey, Ouellet, and Graham describes or suggests applying layers of metal to a nano-element array, where the layers of metal include a substantially continuous layer of an inert metal bonded to the tips of the nano-elements, and where at least a portion of the substantially continuous layer infiltrates at least a portion of the nano- element array. App. Br. 7. Appellants' argument is not persuasive. Zhang teaches growing carbon nanotubes on a substrate (Zhang i-f 24), and then depositing a layer of metal 330, which may include an inert metal such as copper, over the carbon nanotubes array 320 to form a metal matrix around the carbon nanotubes 325 (Id. i-f 25). Accordingly, as shown in Zhang's Figure 3B, the substantially continuous (inert) metal layer 330 in Zhang infiltrates at least a portion of its nano-element array 320. Appellants' argument that Zhang in view of Stacey only teaches infiltration of metal into the nano-element array during rather than prior to the heating and bonding process is also not persuasive. Claim 1 does not require that the infiltration occurs prior to elevating the temperature of the nano-elements, the metal layers, and the substrate. In addition, Appellants bald assertion is not supported by Zhang's disclosure, which appears to teach that infiltration of the nano-element with the continuous (inert) metal layer 330 occurs prior to the heating and bonding process, which would occur once Zhang's free-standing composite structure is attached to other components such as a heat sink using solder. Zhang i-f 28; Fig. 2. 5 Appeal2015-002523 Application 12/359,662 Appellants argue that because Graham teaches reducing adhesion of carbon nanotubes to a growth surface using water/peroxide etching (Graham i-f 27), one of ordinary skill in the art would not have been motivated to combine the teachings of Graham and Zhang. App. Br. 7-8. This argument is not persuasive. The skilled artisan would "be able to fit the teachings of multiple patents together like pieces of a puzzle" since the skilled artisan is "a person of ordinary creativity, not an automaton." KSR Int'! Co. v. Teleflex, Inc., 550 U.S. 398, 420-21 (2007). It is not necessary that the references be physically combinable, without change, to render obvious the invention under review. In re Sneed, 710 F.2d 1544, 1550 (Fed. Cir. 1983). The criterion instead is what these references would have taught or suggested to a person of ordinary skill in the field of the invention. In re Gorman, 933 F.2d 982, 986 (Fed. Cir. 1991). On this record, Appellants do not present persuasive arguments or evidence that one of ordinary skill in the art would not have, through the use of no more than ordinary creativity, modified the applied prior art so as to result in the claimed method. DECISION For the above reasons, the rejection of claims 1-12 is affirmed. No time period for taking any subsequent action in connection with this appeal may be extended under 37 C.F.R. § 1.136(a). AFFIRMED 6 Copy with citationCopy as parenthetical citation