Ex Parte Gillies et alDownload PDFPatent Trial and Appeal BoardFeb 6, 201511175196 (P.T.A.B. Feb. 6, 2015) Copy Citation UNITED STATES PATENT AND TRADEMARK OFFICE _________ BEFORE THE PATENT TRIAL AND APPEAL BOARD __________ Ex parte JENNIFER GILLIES and MARGARET HINES __________ Appeal 2012-009401 Application 11/175,196 Technology Center 2800 ___________ Before ADRIENE LEPIANE HANLON, CATHERINE Q. TIMM, and JAMES C. HOUSEL, Administrative Patent Judges. HANLON, Administrative Patent Judge. DECISION ON APPEAL A. STATEMENT OF THE CASE The Appellants appeal under 35 U.S.C. § 134 from a final rejection of claims 1–4, 6, 7, 10–13, and 22–24 under 35 U.S.C. § 112, first paragraph, based on the written description requirement.1 We have jurisdiction under 35 U.S.C. § 6(b). We AFFIRM. 1 Claims 8, 9, and 14–21 are also pending but have been withdrawn from consideration. Appeal 2012-009401 Application 11/175,196 2 Claims 1 and 13 are the independent claims on appeal. They are reproduced below from the Claims Appendix of the Appeal Brief dated January 30, 2012 (“App. Br.”). The limitation at issue is italicized. 1. A micronized semiconductor nanocrystal complex made by a process comprising: dispersing a plurality of semiconductor nanocrystals colloidally in a solid first matrix material; and micronizing the first matrix material after the dispersing step, such that at least one particle of the micronized semiconductor nanocrystal complex comprises between about 10,000 and about 333 billion semiconductor nanocrystals. App. Br. 11 (emphasis added). 13. A micronized semiconductor nanocrystal complex made by a process comprising: dispersing a plurality of first semiconductor nanocrystals colloidally in a solid first matrix material; dispersing a plurality of second, semiconductor nanocrystals colloidally in a solid second matrix material, wherein the first and second semiconductor nanocrystals are chosen from at least one of: a different size and a different material; and micronizing the first and the second matrix materials after the dispersing steps, such that at least one particle of the micronized semiconductor nanocrystal complex comprises between about 10,000 and about 333 billion semiconductor nanocrystals. App. Br. 12 (emphasis added). The § 112 rejection is sustained for the reasons stated in the Examiner’s Answer dated March 29, 2012 (“Ans.”). We add the following for emphasis. B. DISCUSSION Claims 1 and 13 recite a micronized semiconductor nanocrystal complex made by, inter alia, micronizing a matrix material “such that at least one particle of Appeal 2012-009401 Application 11/175,196 3 the micronized semiconductor nanocrystal complex comprises between about 10,000 and about 333 billion semiconductor nanocrystals.” App. Br. 11, 12. The Examiner finds that “[t]he language of ‘between about 10,000 and about 333 billion’ . . . is not supported by the originally filed disclosure.” Ans. 5. There is no dispute on this record that the claim limitation at issue is not expressly described in the originally filed disclosure. See App. Br. 5 (“no ranges of the number of nanocrystals within a micronized particle are disclosed in the specification”). Nonetheless, the Appellants contend that the claim limitation at issue is “implicitly and/or inherently” supported by the original disclosure. For support, the Appellants rely on “Para. 32 [of the Specification] and the given Examples at Para. 57–62 [of the Specification], as related to the Declarations filed 2/9/10[2] and 6/29/2011.[3]” App. Br. 5. “The test for determining compliance with the written description requirement is whether the disclosure of the application as originally filed reasonably conveys to the artisan that the inventor had possession at that time of the later claimed subject matter.” In re Kaslow, 707 F.2d 1366, 1375 (Fed. Cir. 1983). Compliance with the written description requirement is a question of fact. Ralston Purina Co. v. Far-Mar-Co., Inc., 772 F.2d 1570, 1574 (Fed. Cir. 1985). The Landry and Ballinger Declarations focus on Example 1 in the Appellants’ Specification (Spec. ¶¶ 57, 58) and calculate the number of 2 The Appellants appear to be referring to the Declaration of Mr. Daniel Landry dated February 8, 2010 (hereinafter “Landry Declaration”). The Appellants have included a copy of the Landry Declaration in the Evidence Appendix of the Appeal Brief. 3 Declaration of Dr. Clinton Ballinger dated June 29, 2011 (hereinafter “Ballinger Declaration”). The Appellants have included a copy of the Ballinger Declaration in the Evidence Appendix of the Appeal Brief. Appeal 2012-009401 Application 11/175,196 4 nanocrystals in a micronized particle based on a number of values, including the molecular weight of a PbS nanocrystal, the density of polystyrene, the size of the micronized particle,4 and the size of the nanocrystal.5 Example 1 discloses “a process for preparing a micronized semiconductor nanocrystal complex comprising a plurality of PbS semiconductor nanocrystals in a first matrix material that is polystyrene, wherein the polystyrene is micronized.” Spec. ¶ 57. Example 1 does not disclose the molecular weight of the PbS nanocrystals. Example 1 merely identifies the PbS nanocrystals as “purchased in toluene (Evident Technologies, Troy, New York).” Spec. ¶ 58. Nonetheless, the Appellants argue that, “as described in the Declaration, the molecular weights given to derive the base weight [i.e., the molecular weight of the PbS nanocrystals] are based on calculations of the maximum and minimum sizes of particles given in the specification.”6,7 App. Br. 6 (emphasis added). Turning to the Declarations, Mr. Landry states that the molecular weight for “larger sized nanocrystals” is 600,000 g/mol and the molecular weight for “smaller 4 Example 1 does not specify the size(s) of the micronized particles. See Spec. ¶ 58 (the solid is “micronized to the desired size to form a micronized semiconductor nanocrystal complex”). However, the Appellants disclose that “[t]he particles may be micronized from anywhere between 0.5 microns to 100 microns.” Spec. ¶ 32. 5 The Landry and Ballinger Declarations appear to have been filed in response to a § 103(a) rejection of claims 1, 2, 4, 11–13, 22, and 23 based on Morioka. See Landry Decl. ¶¶ 4–6; Ballinger Decl. ¶¶ 4–6. That rejection is not before us on appeal. 6 The Appellants do not cite to a specific Declaration. For purposes of this appeal, we will assume the Appellants are referring to paragraph 7 of the Landry Declaration and paragraph 8 of the Ballinger Declaration. 7 In the Background of the Invention, the Appellants disclose that “[s]emiconductor nanocrystals are typically tiny crystals of II-VI, III-V, IV-VI materials that have a diameter between 1 nanometer (nm) and 20nm.” Spec. ¶ 3. Appeal 2012-009401 Application 11/175,196 5 nanocrystals” is 20,000 g/mol. Landry Decl. ¶ 7. Dr. Ballinger, on the other hand, states that “[t]he range of possible base molecular weights was from 20,000g/mol to 1,500,000g/mol. These values were the minimum and maximum sizes of the tested nanocrystals, respectively.” Ballinger Decl. ¶ 8 (emphasis added). However, neither Mr. Landry nor Dr. Ballinger correlates the size(s) of the PbS nanocrystals used to calculate the molecular weight with the sizes of nanocrystals disclosed in the Specification. As for the density of the polystyrene, Dr. Ballinger states: Since Polystyrene is a long chain carbon molecule that can vary greatly in length, it is necessary to know the average number of carbons per chain, denoted by Mn, and the average molecular weight per chain, denoted by Mw. The Polystyrene used for this experiment was from Sigma-Aldrich: Product Number: 441147 and Batch Number: 06906TC. The Mw and Mn values from this batch were 350,000 and 170,000 respectively. Ballinger Decl. ¶ 9 (emphasis added); see also App. Br. 7 (“the Polystyrene (Instant Application, Para. 58) used was from Sigma-Aldrich: Product Number 441147 and Batch Number: 06906TC”). However, Example 1 does not identify the polystyrene used. See Spec. ¶ 58. Relying on the calculations in the Landry and Ballinger Declarations, the Appellants contend that the evidence of record shows that the lowest number of nanocrystals per micronized particle is “8.8884E4 (88,884) nanocrystals.” App. Br. 8; compare App. Br. 11, 12 (claims 1 and 13 recite a lower limit of “about 10,000” semiconductor nanocrystals). The Appellants argue: [T]he larger the nanocrystal, the fewer nanocrystals there would be within the micronized particle of the claim. . . . For instance, if a micronized particle of 0.5 microns (Instant Application, Para. 32) was used, which is smaller than the example calculations for a 2 micron particle, and an even larger nanocrystal were used, e.g., molecular Appeal 2012-009401 Application 11/175,196 6 weight greater than 600,000g/mol up to the specified 1,500,000g/mol (Declaration, Point 8)[8], the specified 88,000 nanocrystals (Declaration, Point 9, Paragraph after Equation 7)[9] would support the claimed 10,000 nanocrystals within a micronized particle. App. Br. 8–9 (emphasis added). Suffice it to say that a particle comprising 88,000 nanocrystals does not contain the same number of nanocrystals as a particle comprising as few as about 10,000 nanocrystals. See Ans. 15 (“[t]he number of 10,000 is different from 88,000”). As for the upper limit recited in claims 1 and 13, i.e., “about 333 billion semiconductor nanocrystals,” Dr. Ballinger states: The smallest nanocrystal tested had a molecular weight of 20,000g/mol, while the largest volume was 100 microns in diameter. By using these two variables, the upper limit will yield 3.3332E11 nanocrystals. According to the experiment this would be the upper limit. However, if there were to be error somewhere along the way, and the nanocrystals did not begin to grow with respect to temperature, the smallest crystal size would be that of the unit cell, which is cubic. By using the maximum volume and the molecular weight of the unit cell, the maximum amount of crystals that could exist in a particle would be 2.5239E12 nanocrystals. Ballinger Decl. ¶ 9 (emphasis added). This uncertainty in calculating the maximum number of nanocrystals is further evidence that the originally filed disclosure does not reasonably convey that the Appellants had possession of the claimed range at the time the instant Application was filed. 8 We understand the Appellants to be referring to paragraph 8 of the Ballinger Declaration. 9 We understand the Appellants to be referring to paragraph 9 of the Ballinger Declaration. Appeal 2012-009401 Application 11/175,196 7 For the reasons set forth above and in the Examiner’s Answer, the Examiner’s finding that the originally filed disclosure does not provide written description support for the claim limitation “between about 10,000 and about 333 billion semiconductor nanocrystals” is supported by a preponderance of the evidence. C. DECISION The decision of the Examiner is affirmed. No time period for taking any subsequent action in connection with this appeal may be extended under 37 C.F.R. § 1.136(a)(1). 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