Ex Parte Bour et alDownload PDFPatent Trial and Appeal BoardSep 11, 201511552474 (P.T.A.B. Sep. 11, 2015) Copy Citation UNITED STATES PATENT AND TRADEMARK OFFICE UNITED STATES DEPARTMENT OF COMMERCE United States Patent and Trademark Office Address: COMMISSIONER FOR PATENTS P.O. Box 1450 Alexandria, Virginia 22313-1450 www.uspto.gov APPLICATION NO. FILING DATE FIRST NAMED INVENTOR ATTORNEY DOCKET NO. CONFIRMATION NO. 11/552,474 10/24/2006 David Bour 011203 USA/NBD/NEON/ESONG 2128 45401 7590 09/14/2015 BLAKELY SOKOLOFF TAYLOR & ZAFMAN LLP 1279 Oakmead Parkway Sunnyvale, CA 94085-4040 EXAMINER CHEN, KEATH T ART UNIT PAPER NUMBER 1716 MAIL DATE DELIVERY MODE 09/14/2015 PAPER Please find below and/or attached an Office communication concerning this application or proceeding. The time period for reply, if any, is set in the attached communication. PTOL-90A (Rev. 04/07) UNITED STATES PATENT AND TRADEMARK OFFICE ________________ BEFORE THE PATENT TRIAL AND APPEAL BOARD ________________ Ex parte DAVID BOUR1 and Lori D. Washington ________________ Appeal 2013-007605 Application 11/552,474 Technology Center 1700 ________________ Before BEVERLY A. FRANKLIN, MARK NAGUMO, and N. WHITNEY WILSON, Administrative Patent Judges. NAGUMO, Administrative Patent Judge. DECISION ON APPEAL David Bour and Lori D. Washington (“Bour”) timely appeal under 35 U.S.C. § 134(a) from the Final Rejection2 of claims 25–35, which are all of the pending claims. We have jurisdiction. 35 U.S.C. § 6. We affirm. 1 The real party in interest is listed as Applied Materials, Inc. (Appeal Brief, filed 4 February 2013 (“Br.”), 3.) 2 Office action mailed 3 April 2012 (“Final Rejection”; cited as “FR”). Appeal 2013-007605 Application 11/552,474 2 OPINION A. Introduction3 The subject matter on appeal relates to an apparatus for metal-organic chemical vapor deposition (“MOCVD”) of “III-V nitride films” from volatile group III precursors such as trimethylgallium (“TMGa”) or trimethylaluminum (“TMAl”) and a nitrogen precursor such as ammonium. (Spec. 1 [0003].) The various steps of the process are said to occur at varied temperatures, and it is said to be desirable to provide a susceptor (i.e., a wafer support) capable of temperature changes greater than 10°C/s, significantly more rapid than conventional temperature ramping, which is said to be less than about 5°C/s. (Id. at 10 [0039].) In addition to the faster processing and increased throughput (id. at 3–4, [0018]–[0019]), the faster temperature changes are said to result in improvements in the levels of impurities at growth stop interfaces (id. at 2–3 [0011]) and in the structural quality of the deposited structures (id. at 4 [0021]). Sole independent claim 25 is representative of the dispositive issues and reads: A semiconductor processing unit comprising: a chamber [215] having walls; a susceptor [208] located within said chamber, said susceptor formed from a material having a low thermal mass; a substrate receiving region [~209] located on said susceptor; 3 Application 11/552,474, Substrate support structure with rapid temperature change, filed 24 October 2006. We refer to the “ʼ474 Specification,” which we cite as “Spec.” Appeal 2013-007605 Application 11/552,474 3 a gas distribution structure [221] located above and over said substrate receiving region for providing source gases into said chamber; a gas reaction area [216] located above and over, and separate from, said substrate receiving region, between said gas distribution structure and said substrate receiving region, said gas reaction area for forming deposition products for said substrate receiving region, wherein said susceptor is for changing a temperature of said gas reaction area at a rate greater than 10°C/sec; a heat exchanger for limiting formation of said deposition products on the walls of said chamber; and a plurality of lamp heating elements for uniformly heating said susceptor. (Claims App., Br. 15; some indentation, paragraphing, emphasis, and bracketed labels to elements shown in Fig. 2, reproduced below, added.) {Fig. 2 is said to shows an exemplary CVD system} Appeal 2013-007605 Application 11/552,474 4 As shown in Fig. 2, enclosure assembly 2374 contains evacuable deposition chamber 215, which holds susceptor 208 having a substrate receiving region for substrate 209 and that may have controllably moveable heaters 226. (Spec. 5 [0024].) In other embodiments, lamp heaters may be placed in various locations to heat the substrate support structure rapidly. (Id. at 6 [0026].) The ʼ474 Specification teaches that susceptor 208 is formed from low thermal mass materials such as nickel-iron alloy, quartz, silicon, silicon carbide, or carbon composite. (Id. at 9 [0034].) According to the Specification, “thermal mass is a measure of the thermal energy needed to raise a unit mass by one Kelvin.” (Id. at [0035].) Reactive gases and carrier gases (id. at 6 [0028]), as well as purge gases, are introduced via vapor delivery system 220 through gas distribution structure 221 to gas reaction area 216 above and over substrate 209 (id. at 5 [0025]). When a liquid source is used for the reactive gases, the gas delivery system is said to include “a liquid injection system or other appropriate mechanism (e.g., a bubbler) to vaporize the liquid.” (Id. at 7 [0028].) The walls of the deposition chamber 215 can be heated or cooled by circulating a heat-exchange liquid through channels (not shown). (Id. at 7 [0030].) Heating the walls is said to reduce or eliminate condensation of undesirable reaction products on the walls of chamber 215. (Id.) Moreover, in the words of the ʼ474 Specification, “a cool liquid may be used to remove heat from the system during other [non-thermal 4 Throughout this Opinion, for clarity, labels to elements in figures are presented in bold font, regardless of their presentation in the original document. Appeal 2013-007605 Application 11/552,474 5 deposition] processes, or to limit formation of deposition products on the walls of the chamber.” (Id.) The Examiner maintains the following grounds of rejection:5, 6 A. Claims 25–30, and 35 stand rejected under 35 U.S.C. § 103(a) in view of the combined teachings of Moore,7 Nulman,8 Ballance,9 and Johnsgard.10 A1. Claims 31–34 stand rejected under 35 U.S.C. § 103(a) in view of the combined teachings of Moore, Nulman, Ballance, Johnsgard, and Sverdlov.11 5 Examiner’s Answer mailed 22 February 2013 (“Ans.”). 6 The Examiner has withdrawn a rejection of claims 25–35 under 35 U.S.C. § 112(1), for lack of written description of the gas reaction area. (Ans. 6, ll. 6–12.) 7 Gary M. Moore, Multi-layer susceptor for rapid thermal process reactors, U.S. Patent No. 5,820,686 (1998). 8 Jaim Nulman and Dan Maydan, Wafer heating and monitor module and method of operation, U.S. Patent No. 5,098,198 (1992). We include Nulman, which the Examiner (FR 3, ll. 7–9) and Bour (Br. 9, 10, 12) cite, in the statement of rejection for completeness. 9 David S. Ballance et al., Gas introduction showerhead for an RTP chamber with upper and lower transparent plates and gas flow therebetween, U.S. Patent No. 5,781,693 (1998). 10 Kristian E. Johnsgard and James McDiarmid, Thermal processing system with supplemental resistive heater and shielded optical pyrometry, U.S. Patent No. 5,830,277 (1998). 11 Boris N. Sverdlov and Jo Stephen Major, Jr., Method of doping GaN layers P-type for device fabrication, U.S. Patent No. 5,888,886 (1999). Appeal 2013-007605 Application 11/552,474 6 B. Discussion Findings of fact throughout this Opinion are supported by a preponderance of the evidence of record. Bour argues the rejection of claims 25–30 and 35 as a group. (Br. 9-11.) Thus, these claims stand or fall with claim 25. 37 C.F.R. § 41.37(c)(1)(iv) (2012). Bour urges that the inventors “teach and claim a gas reaction area separate from a substrate receiving region. A gas reaction area is an area where source gases are reacted together to form a deposition product which is only then grown on a wafer in a substrate receiving region above the susceptor.” (Br. 10, ll. 12–15.) In contrast, Moore and Nulman, in Bour’s view, teach a Rapid Thermal Process (“RTP”) apparatus in which an anneal gas, such as N2 or Ar, is flowed into the chamber for direct contact with a heated wafer. Neither reference, according to Bour, teaches or suggests the susceptor provided “for changing a temperature of the gas reaction area at a rate greater than 10°C/sec” that is required by the appealed claims. (Id. at ll. 20-24.) Bour acknowledges that Ballance describes a showerhead in an RTP chamber that makes possible CVD in an RTP chamber. (Id. at 11, ll. 1–3.) However, in Bour’s view, “Ballance at least does not disclose a distinct gas reaction area above a substrate receiving region, and, thus, fails to cure the above noted deficiencies of Moore.” (Id. at 11, ll. 3–5.) These arguments are not persuasive of harmful error in the appealed rejection. The claims are drawn to an apparatus, not to a process, and the critical limitations are in functional form. That is, rather than reciting structure, they recite functions that various parts of the apparatus must Appeal 2013-007605 Application 11/552,474 7 perform, such as the susceptor that must change the temperature of the gas reaction area at a rate greater than 10°C/s. As the predecessor to our reviewing court instructed, such functional characterizations are not improper in claims, but “‘[f]unctional’ terminology may render a claim quite broad. By its own literal terms a claim employing such language covers any and all embodiments which perform the recited function.” In re Swinehart, 439 F.2d 210, 213 (CCPA 1971). Fig. 1, of Ballance, below, illustrates an RTP chamber. {Ballance, Fig. 1, shows an RTP chamber 10} Ballance, Fig. 1, shows an RTP chamber 10 with processing cavity 14 between bottom plate 52 and substrate 16. Gas supplied to tubes 48 flows out of bottom plate 52 through holes 60 (see arrows). Comparison of Fig. 2 of the ʼ474 Specification, reproduced supra, with Ballance Fig. 1, shows the strong structural correspondence of processing cavity 14, which is above and Appeal 2013-007605 Application 11/552,474 8 over the substrate 16, and beneath the gas distribution structure, with the recited “gas reaction area” [216]. On the present record, Bour’s arguments that the alleged failure of Ballance to describe a specific version of chemical vapor deposition in which the gaseous reactants react in a gas reaction area (rather than, e.g., on the substrate) are not persuasive of harmful error. Ballance teaches “[t]he invention makes it possible to perform CVD in an RTP chamber in which the substrate is heated by lamp radiation from the top side of the substrate.” (Ballance, col. 2, ll. 54–56.) Bour has not explained why this teaching would not have suggested that the lamp-illuminated RTP chambers could be modified for use as CVD chambers. Nor has Bour explained why Moore’s teaching that “[t]he RTP reactor typically can heat the wafer or wafers at a rate between 10°C./sec and 400°C./sec” (Moore, col. 8, ll. 30–31), cited by the Examiner (FR 6, l. 3; Ans. 4, ll. 22) would not have suggested the heating rate limitation required by claim 25. Bour argues that Johnsgard does not cure the defects of Moore and Ballance (Br. 11, 2d para.). Not having been persuaded of harmful error in the findings of fact regarding Moore and Ballance, we are not persuaded of error in the further determinations based on Johnsgard regarding the heat exchanger for the walls. Bour argues that the p-type layer process described by Sverdlov would not have been applied to the RTP process described by Moore and Nulman, and that therefore the rejection of claims 31–34 should be reversed. (Id. at para. bridging 11–12). This argument is misdirected as the Examiner Appeal 2013-007605 Application 11/552,474 9 has relied on Ballance as evidence that an RTP apparatus modified to conduct CVD processes as recited in claim 25 would have been obvious. Bour argues further that the susceptor of an RTP apparatus may be used to control the temperature of the substrate, whereas in the claimed apparatus, the temperature of an overlying gas reaction area is controlled by the susceptor. (Br. 12, l. 11, to 13, l. 5.) Bour has not, however, directed our attention to any description in the ʼ474 Specification indicating how the temperature of the gas reaction area is controlled in a way that is distinct in the claimed apparatus compared to any of the prior art apparatuses. Nor has Bour discussed, let alone rebutted, the Examiner’s findings (FR 4, ll. 9–12; Ans. 3, ll. 29–32) regarding the heating of that area. Thus, to the extent Bour is arguing that heating the substrate is somehow distinct from heating the gas reaction area, that argument is not supported by sufficient credible evidence of record. We decline to credit such unsupported attorney argument as to issues of fact. Not being persuaded of harmful error in the appealed rejections, we affirm. C. Order It is ORDERED that the rejection of claims 25–35 is affirmed. No time period for taking any subsequent action in connection with this appeal may be extended under 37 C.F.R. § 1.136(a). AFFIRMED cdc Copy with citationCopy as parenthetical citation