Ex Parte an et alDownload PDFPatent Trial and Appeal BoardDec 27, 201612879578 (P.T.A.B. Dec. 27, 2016) Copy Citation United States Patent and Trademark Office UNITED STATES DEPARTMENT OF COMMERCE United States Patent and Trademark Office Address: COMMISSIONER FOR PATENTS P.O.Box 1450 Alexandria, Virginia 22313-1450 www.uspto.gov APPLICATION NO. FILING DATE FIRST NAMED INVENTOR ATTORNEY DOCKET NO. CONFIRMATION NO. 12/879,578 09/10/2010 CHONG Pyung An SP10-203 7261 22928 7590 12/29/2016 TORNTNO TNmRPORATFD EXAMINER SP-TI-3-1 AUER, LAURA A CORNING, NY 14831 ART UNIT PAPER NUMBER 1783 NOTIFICATION DATE DELIVERY MODE 12/29/2016 ELECTRONIC Please find below and/or attached an Office communication concerning this application or proceeding. The time period for reply, if any, is set in the attached communication. Notice of the Office communication was sent electronically on above-indicated "Notification Date" to the following e-mail address(es): u sdocket @ corning .com PTOL-90A (Rev. 04/07) UNITED STATES PATENT AND TRADEMARK OFFICE BEFORE THE PATENT TRIAL AND APPEAL BOARD Ex parte CHONG PYUNG AN and MARK ALEJANDRO QUESDA Appeal 2015-006547 Application 12/879,578 Technology Center 1700 Before ADRIENE LEPIANE HANLON, MICHAEL P. COLAIANNI, and MICHAEL G. McMANUS, Administrative Patent Judges. COLAIANNI, Administrative Patent Judge. DECISION ON APPEAL Appeal 2015-006547 Application 12/879,578 Appellants appeal under 35 U.S.C. § 134 the final rejection of claims 1 and 3-13. We have jurisdiction over the appeal pursuant to 35 U.S.C. § 6(b). We AFFIRM. Appellants’ invention is directed to hermetic barrier layers that are self-passivating, inorganic, and mechanically stable hermetic thin films (Spec. 12). Claim 1 is illustrative: 1. A hermetic thin film, comprising: a first inorganic layer having an initial thickness formed over a substrate; and a second inorganic layer contiguous with the first inorganic layer; wherein the first inorganic layer is amorphous; the second inorganic layer consists essentially of an oxidation and/or hydrolysis reaction product of the first inorganic layer; a molar volume of the second inorganic layer is from about -1% to 15% greater than a molar volume of the first inorganic layer; and an equilibrium thickness of the second inorganic layer is at least 10% of but less than the initial thickness of the first inorganic layer. Appellants appeal the following rejections: 1. Claims 1, 3, and 7-12 are rejected under 35 U.S.C. § 102(b) as unpatentable over Aitken (US 2007/0252526 Al, pub. Nov. 1, 2007). 2 Appeal 2015-006547 Application 12/879,578 2. Claims 4-6 and 13 are rejected under 35 U.S.C. § 103(a) as unpatentable over Aitken in view of Zimmerman (US 2008/0305355 Al, pub. Dec. 11, 2008). With regard to rejection (1), Appellants’ arguments focus on claims 1, 9, and 10 only (App. Br. 5-10). Appellants’ arguments regarding claims 4-6 under rejection (2) are the same arguments made with regard to rejection (1) (App. Br. 11). Accordingly, claims 3-12 will stand or fall with our analysis of the rejection of claim 1. Claim 13 under rejection (2) is argued separately (App Br. 11-12). FINDINGS OF FACT & ANALYSIS REJECTION (1): § 102(b) Claim 1 The Examiner finds that Aitken teaches the subject matter of claim 1 with the requirement that the second layer is contiguous with the first inorganic layer, the range of molar volume of the second inorganic layer, and the thickness of the first inorganic layer being at least 10% being inherent properties of Aitken’s product (Final Act. 2-3). The Examiner finds that Aitken uses the same sealing material (tin fluorophosphate) and a similar process as Appellants’ material and process, respectively, where the sealing material is exposed to air (Final Act. 3; Ans. 4-5). The Examiner finds that Aitken discloses cooling the device to be coated, applying a coating over the device and then heat-treating the device at a temperature and environment that does not damage the inner layers of device (Ans. 3-4, Fig. 2). The Examiner finds that Aitken’s heat-treatment step may be 3 Appeal 2015-006547 Application 12/879,578 carried out in a vacuum “if desired” (Ans. 4). The Examiner finds that Aitken’s teaching that a vacuum or oxygen-free environment may be used “if desired” means that ambient air or other environment may be used during the heat-treatment step (Ans. 4). The Examiner finds that when the deposited coating, which is the same material disclosed by Appellants as a suitable coating (tin fluorophosphate), is exposed to air, the coating would react with the oxygen in the air and form an oxidized layer on the coating which has the same properties as claimed by Appellants (Ans. 4-5). Appellants argue that Aitken’s process that uses a heat-treatment step is different than Appellants’ method of forming the hermetic thin film where no heat treatment step is used (App. Br. 7). Appellants argue that Aitken uses a heat-treatment step which is performed in an inert atmosphere or vacuum to help ensure that a water and oxygen-free condition is maintained throughout the entire sealing process. (App. Br. 7). Regarding claims 1, 9, and 10, Appellants argue that Figure 4 of Aitken and the discussion of Figure 4 in 136 evince that a suitable oxidation profile of the hermetic seals (i.e., 100c in Fig. 4) has a low oxidation profile (less than 10% oxidation) for over 1000 hours in the accelerated-aging test (App. Br. 7). Appellants contend that during the heat-treatment the layer is consolidated so that the pores in the layer are removed and the layer has improved resistance to oxidation (App. Br. 8). Appellants argue that the heat-treated layer would result in a film that has a limited capacity for oxidation (App. Br. 8). Appellants argue that in light of these arguments the Examiner has not established that Aitken’s hermetic sealing layer has the properties recited in the claim. Id. Appellants argue that Aitken’s “if desired” language in 121 does not disclose that the heat-treatment step is optional (Reply Br. 5). 4 Appeal 2015-006547 Application 12/879,578 Appellants’ arguments are not persuasive because they fail to show reversible error with the Examiner’s stated rejection. The Examiner finds that Aitken teaches that the use of an inert gas or a vacuum during the heat- treatment is optional (“if desired”), not that the heat-treatment step is optional (Ans. 4). In other words, the Examiner finds that Aitken teaches that the heat-treatment could be performed in other environments including ambient air. Id. Appellants do not specifically contest this finding of the Examiner with regard to Aitken’s 121 disclosure. The Examiner reasonably establishes that performing Aitken’s heat-treatment in air would have reasonably been expected to form an oxide layer on the tin fluorophosphate layer. Indeed, Appellants teach that the reaction of tin fluorophosphate and oxygen spontaneously occurs (Spec. Tflf 16, 35). Appellants further disclose that oxidation of the inorganic coating layer may occur by exposing the coating to “steam” (Spec. 121). Steam is vapor from water heated above its boiling point (i.e., 100°C). In other words, Appellants own disclosure may use an elevated temperature to react the oxygen containing environment and inorganic layer. Appellants’ arguments regarding Aitken’s Figure 4 as applied to claims 1, 9, and 10 are not accurate. The Examiner finds that Aitken’s Figure 4 shows the oxidation of the calcium test patch that is sealed underneath the hermetic coating (Aitken H 35, 36; Ans. 6). Accordingly, the 10% oxidation shown in Figure 4 with respect to sample 100c refers to oxidation of the underlying calcium patch, not oxidation of the tin fluorophosphate film coating the patch. Appellants argue that the Examiner has improperly read limitations regarding the inorganic coating material into the claims (App. Br. 9). 5 Appeal 2015-006547 Application 12/879,578 Appellants contend that claim 1 is not limited to any particular inorganic material and the Examiner cherry-picked the tin fluorophosphate material from the list of materials. Id. Therefore, Appellants contend that the Examiner has not established that claimed properties are necessarily present in Aitken’s hermetic film. Id. The Examiner has not read limitations into the claims. Rather, the Examiner construed the claim phrase “inorganic layer” in claim 1 as including Appellants’ disclosed tin fluorophosphate (Final Act. 3). In other words, the claim is not limited to any particular inorganic layer material and the Examiner finds that Aitken’s teaching to use tin fluorophosphate satisfies properly construed claim 1. REJECTION (2): § 103 Claim 13 Appellants argue that the Examiner relied on Zimmerman’s hermetic copper oxide material as inherently having the molar volume and thickness properties (App. Br. 11-12). Appellants argue that Zimmerman’s process is completely different than Appellants’ process used to form the hermetic thin film. Id. Appellants argue that Zimmerman’s cupric oxide layer is crystalline and does not teach or suggest a hermetic thin film having an amorphous first inorganic layer (App. Br. 12). Appellants’ arguments are unpersuasive because they fail to address the Examiner’s stated rejection. The Examiner finds that Aitken teaches the general process for forming a hermetic thin film, but fails to teach the inorganic layer is an oxide of copper (Final Act. 5-6). The Examiner finds that Zimmerman teaches that an oxide of copper is a known hermetic layer (Final Act. 6). The Examiner finds that Zimmerman and Aitken teach 6 Appeal 2015-006547 Application 12/879,578 material sufficient for forming a hermetic seal (Ans. 6). The Examiner concludes that it would have been obvious to use Zimmerman’s copper oxide as the inorganic material in Aitken’s hermetically sealed device as an alternative inorganic, hermetically sealing material (Final Act. 7; Ans. 6). The Examiner is not proposing to bodily incorporate Zimmerman’s process of treating the copper oxide material to form a hermetic seal to form Aitken’s hermetically sealed device. Instead the Examiner is proposing to substitute Zimmerman’s copper oxide inorganic material as the hermetic sealing material in Aitken’s device. In other words, Zimmerman’s copper oxide would have been used in Aitken’s process for forming the hermetic sealing layer. As noted above in our discussion of Aitken under the § 102 rejection, we find that the Examiner has put forth enough evidence that using Aitken’s process, as modified by Zimmerman, to form the inorganic layers would have inherently resulted in a layer having the properties recited in the claims. On this record, we affirm the Examiner’s § 102 rejection over Aitken and § 103 rejection over Aitken in view of Zimmerman. DECISION The Examiner’s decision is affirmed. No time period for taking any subsequent action in connection with this appeal may be extended under 37 C.F.R. § 1.136(a)(1). ORDER AFFIRMED 7 Copy with citationCopy as parenthetical citation